3-(1-{3-[(tert.-butoxycarbonyl)amino]propyl}-1H-indol-3-yl)-4-(3,4,5-trimethoxyphenyl)-maleinimide

Base Information

Chemical Name:3-(1-{3-[(tert.-butoxycarbonyl)amino]propyl}-1H-indol-3-yl)-4-(3,4,5-trimethoxyphenyl)-maleinimide
CAS No.:1312545-37-1
Molecular Formula:C₂₉H₃₃N₃O₇
Molecular Weight:535.597
Hs Code.:

Synonyms:3-(1-{3-[(tert.-butoxycarbonyl)amino]propyl}-1H-indol-3-yl)-4-(3,4,5-trimethoxyphenyl)-maleinimide

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Chemical Property of 3-(1-{3-[(tert.-butoxycarbonyl)amino]propyl}-1H-indol-3-yl)-4-(3,4,5-trimethoxyphenyl)-maleinimide

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Technology Process of 3-(1-{3-[(tert.-butoxycarbonyl)amino]propyl}-1H-indol-3-yl)-4-(3,4,5-trimethoxyphenyl)-maleinimide

There total 4 articles about 3-(1-{3-[(tert.-butoxycarbonyl)amino]propyl}-1H-indol-3-yl)-4-(3,4,5-trimethoxyphenyl)-maleinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1312545-36-0
ethyl-2-(1-{3-[(tert.-butoxycarbonyl)amino]propyl}-1H-indol-3-yl)-2-oxoacetate

: 91248-14-5
2-(3,4,5-trimethoxyphenyl)acetamide

: 1312545-37-1
3-(1-{3-[(tert.-butoxycarbonyl)amino]propyl}-1H-indol-3-yl)-4-(3,4,5-trimethoxyphenyl)-maleinimide

Guidance literature:: With potassium tert-butylate;

Reference yield: 36.8%

: 1312545-37-1
3-(1-{3-[(tert.-butoxycarbonyl)amino]propyl}-1H-indol-3-yl)-4-(3,4,5-trimethoxyphenyl)-maleinimide

Guidance literature:: With potassium tert-butylate;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1312545-37-1
3-(1-{3-[(tert.-butoxycarbonyl)amino]propyl}-1H-indol-3-yl)-4-(3,4,5-trimethoxyphenyl)-maleinimide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate; potassium bromide / chloroform; water / 5 h / Reflux

2: caesium carbonate / N,N-dimethyl-formamide / 8 h / 75 - 80 °C / Inert atmosphere

3: potassium tert-butylate

With potassium tert-butylate; sodium hydrogencarbonate; caesium carbonate; potassium bromide; In chloroform; water; N,N-dimethyl-formamide;