p-tolyl 3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-1-thio-β-L-fucopyranoside

Base Information

Chemical Name:p-tolyl 3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-1-thio-β-L-fucopyranoside
CAS No.:1419180-45-2
Molecular Formula:C₂₄H₃₀O₅S
Molecular Weight:430.565
Hs Code.:

Synonyms:p-tolyl 3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-1-thio-β-L-fucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-tolyl 3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-1-thio-β-L-fucopyranoside

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Technology Process of p-tolyl 3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-1-thio-β-L-fucopyranoside

There total 1 articles about p-tolyl 3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-1-thio-β-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 4-methylphenyl 3,4-O-isopropylidine-1-thio-β-L-fucopyranoside

: 824-94-2
p-methoxybenzyl chloride

: 1419180-45-2
p-tolyl 3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-1-thio-β-L-fucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 4h;
DOI:10.1039/c2ra22407k

Reference yield: 83.0%

: 1419180-43-0
p-methoxyphenyl 3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1→3)-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 1419180-45-2
p-tolyl 3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-1-thio-β-L-fucopyranoside

: 1419180-46-3
p-methoxyphenyl 3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1→3)-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; silica-gel-supported sulfuric acid; In dichloromethane; at -40 ℃; for 1.5h; diastereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1039/c2ra22407k