Technology Process of C27H32ClNO4
There total 8 articles about C27H32ClNO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
water; ethyl acetate;
at 0 ℃;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C
1.2: 0 °C
2.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0 °C
3.1: hydrogenchloride / tetrahydrofuran; water / 80 °C
4.1: water / 6 h / 0 - 60 °C
5.1: water; potassium hydroxide / Inert atmosphere; Reflux
5.2: 0 - 10 °C / pH 2
6.1: thionyl chloride / 8.5 h / 0 - 40 °C / Inert atmosphere
7.1: sodium hydroxide / water; ethyl acetate / 0 °C
With
hydrogenchloride; thionyl chloride; dimethylsulfide borane complex; water; methanesulfonyl chloride; triethylamine; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride / tetrahydrofuran; water / 80 °C
2.1: water / 6 h / 0 - 60 °C
3.1: water; potassium hydroxide / Inert atmosphere; Reflux
3.2: 0 - 10 °C / pH 2
4.1: thionyl chloride / 8.5 h / 0 - 40 °C / Inert atmosphere
5.1: sodium hydroxide / water; ethyl acetate / 0 °C
With
hydrogenchloride; thionyl chloride; water; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; water; ethyl acetate;