{3-[2,6-dibromo-4-(2-tert-butoxycarbonylamino-ethyl)-phenoxy]-propyl}-methyl-carbamic acid methyl ester

Base Information

Chemical Name:{3-[2,6-dibromo-4-(2-tert-butoxycarbonylamino-ethyl)-phenoxy]-propyl}-methyl-carbamic acid methyl ester
CAS No.:958255-22-6
Molecular Formula:C₁₉H₂₈Br₂N₂O₅
Molecular Weight:524.25
Hs Code.:

{3-[2,6-dibromo-4-(2-<i>tert</i>-butoxycarbonylamino-ethyl)-phenoxy]-propyl}-methyl-carbamic acid methyl ester

Synonyms:{3-[2,6-dibromo-4-(2-tert-butoxycarbonylamino-ethyl)-phenoxy]-propyl}-methyl-carbamic acid methyl ester

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Chemical Property of {3-[2,6-dibromo-4-(2-tert-butoxycarbonylamino-ethyl)-phenoxy]-propyl}-methyl-carbamic acid methyl ester

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Technology Process of {3-[2,6-dibromo-4-(2-tert-butoxycarbonylamino-ethyl)-phenoxy]-propyl}-methyl-carbamic acid methyl ester

There total 9 articles about {3-[2,6-dibromo-4-(2-tert-butoxycarbonylamino-ethyl)-phenoxy]-propyl}-methyl-carbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 954100-52-8
methyl (3-bromopropyl)methylcarbamate

: 210880-88-9
N-(tert-butoxycarbonyl)-3,5-dibromo-4-hydroxy-β-phenethylamine

: 958255-22-6
{3-[2,6-dibromo-4-(2-tert-butoxycarbonylamino-ethyl)-phenoxy]-propyl}-methyl-carbamic acid methyl ester

Guidance literature:: With potassium carbonate; In acetone; for 12h; Heating;

Reference yield:

: 958255-17-9
methyl (3-hydroxypropyl)(methyl)carbamate

: 958255-22-6
{3-[2,6-dibromo-4-(2-tert-butoxycarbonylamino-ethyl)-phenoxy]-propyl}-methyl-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / phosphorus tribromide / diethyl ether / 0.5 h / 20 °C

2: 86 percent / K₂CO₃ / acetone / 12 h / Heating

With phosphorus tribromide; potassium carbonate; In diethyl ether; acetone;

Reference yield:

: 958255-19-1
2-[3,5-dibromo-4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-ethanol

: 958255-22-6
{3-[2,6-dibromo-4-(2-tert-butoxycarbonylamino-ethyl)-phenoxy]-propyl}-methyl-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: 82 percent / triethylamine / CH₂Cl₂ / 3 h / cooling

2.1: 86 percent / sodium azide / dimethylformamide / 4 h / Heating

3.1: triphenylphosphine / methanol / 4 h / 20 °C

3.2: 85 percent / methanol / 4 h

4.1: 80 percent / tetrabutylammonium fluoride / methanol / 3 h

5.1: 86 percent / K₂CO₃ / acetone / 12 h / Heating

With sodium azide; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; triphenylphosphine; In methanol; dichloromethane; N,N-dimethyl-formamide; acetone;