ethyl <6-amino-4-<<2-(4-hydroxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

Base Information

Chemical Name:ethyl <6-amino-4-<<2-(4-hydroxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime
CAS No.:139016-59-4
Molecular Formula:C₁₇H₂₀N₆O₆
Molecular Weight:404.382
Hs Code.:

Synonyms:ethyl <6-amino-4-<<2-(4-hydroxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

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Chemical Property of ethyl <6-amino-4-<<2-(4-hydroxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

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Technology Process of ethyl <6-amino-4-<<2-(4-hydroxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

There total 5 articles about ethyl <6-amino-4-<<2-(4-hydroxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60-29-7,927820-24-4
diethyl ether

: 141574-37-0
2-amino-4'-hydroxypropiophenone oxime

: 139016-59-4
ethyl <6-amino-4-<<2-(4-hydroxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

Guidance literature:: With triethylamine; In isopropyl alcohol;

Reference yield:

: 53946-87-5
2-bromo-(4'-hydroxyphenyl)-propan-1-one

: 139016-59-4
ethyl <6-amino-4-<<2-(4-hydroxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

Guidance literature:: Multi-step reaction with 4 steps

1: 640 mg / sodium azide / H₂O; methanol / 16 h / Ambient temperature

2: 438 mg / hydroxylamine hydrochloride, pyridine / ethanol / 6 h / Heating

3: 4.3 g / H₂ / Raney nickel / ethanol / 760 Torr

4: 1.49 g / Et₃N / propan-2-ol / 6 h / Heating

With pyridine; sodium azide; hydroxylamine hydrochloride; hydrogen; triethylamine; nickel; In methanol; ethanol; water; isopropyl alcohol;
DOI:10.1021/jm00084a003

Reference yield:

: 141574-35-8
2-Azido-1-(4-hydroxy-phenyl)-propan-1-one

: 139016-59-4
ethyl <6-amino-4-<<2-(4-hydroxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 438 mg / hydroxylamine hydrochloride, pyridine / ethanol / 6 h / Heating

2: 4.3 g / H₂ / Raney nickel / ethanol / 760 Torr

3: 1.49 g / Et₃N / propan-2-ol / 6 h / Heating

With pyridine; hydroxylamine hydrochloride; hydrogen; triethylamine; nickel; In ethanol; isopropyl alcohol;
DOI:10.1021/jm00084a003