4,6-di-O-acetyl-3-azido-2-O-benzyl-3-deoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxydibekacin

Base Information

Chemical Name:4,6-di-O-acetyl-3-azido-2-O-benzyl-3-deoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxydibekacin
CAS No.:959919-45-0
Molecular Formula:C₅₇H₆₉N₇O₁₉S₄
Molecular Weight:1284.47
Hs Code.:

Synonyms:4,6-di-O-acetyl-3-azido-2-O-benzyl-3-deoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxydibekacin

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Chemical Property of 4,6-di-O-acetyl-3-azido-2-O-benzyl-3-deoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxydibekacin

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Technology Process of 4,6-di-O-acetyl-3-azido-2-O-benzyl-3-deoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxydibekacin

There total 2 articles about 4,6-di-O-acetyl-3-azido-2-O-benzyl-3-deoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxydibekacin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 959918-62-8
4,6-di-O-acetyl-3-azido-2-O-benzyl-1-bromo-3-deoxy-α-D-glucopyranose

: 959919-44-9
3',4'-dideoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxyneamine

: 959919-45-0
4,6-di-O-acetyl-3-azido-2-O-benzyl-3-deoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxydibekacin

Guidance literature:: 4,6-di-O-acetyl-3-azido-2-O-benzyl-1-bromo-3-deoxy-α-D-glucopyranose; 3',4'-dideoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxyneamine; In dichloromethane; at 20 ℃; for 3h; Drierite;

With mercury(II) cyanide; In dichloromethane; at 20 ℃; for 104h; Product distribution / selectivity; light shielding;

Reference yield: 27.0%

: 959918-63-9
phenyl 4,6-di-O-acetyl-3-azido-2-O-benzyl-3-deoxy-1-thio-α-D-glucopyranoside

: 959919-44-9
3',4'-dideoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxyneamine

: 959919-45-0
4,6-di-O-acetyl-3-azido-2-O-benzyl-3-deoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxydibekacin

Guidance literature:: phenyl 4,6-di-O-acetyl-3-azido-2-O-benzyl-3-deoxy-1-thio-α-D-glucopyranoside; 3',4'-dideoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxyneamine; In dichloromethane; at 20 ℃; for 1h; Molecular sieve;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -20 ℃; for 15h; Product distribution / selectivity; light shielding;

Reference yield: 94.0%

: 959919-45-0
4,6-di-O-acetyl-3-azido-2-O-benzyl-3-deoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxydibekacin

: 959919-46-1
3-azido-2-O-benzyl-3-deoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxydibekacin

Guidance literature:: 4",6"-di-O-acetyl-3"-azido-2"-O-benzyl-3"-deoxy-5-epi-1,3,2',6'-tetra-N-tosyl-2-hydroxydibekacin; With sodium methylate; In methanol; at 20 ℃; for 1h;

In methanol;