N-(2-phenyl-2-oxoethyl)<<(2,4-dioxo-1-imidazolidinyl)imino>methyl>formamide

Base Information

• Chemical Name: N-(2-phenyl-2-oxoethyl)<<(2,4-dioxo-1-imidazolidinyl)imino>methyl>formamide
• CAS No.: 64748-75-0
• Molecular Formula: C₁₃H₁₂N₄O₄
• Molecular Weight: 288.263

Synonyms:N-(2-phenyl-2-oxoethyl)<<(2,4-dioxo-1-imidazolidinyl)imino>methyl>formamide

Chemical Property of N-(2-phenyl-2-oxoethyl)<<(2,4-dioxo-1-imidazolidinyl)imino>methyl>formamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of N-(2-phenyl-2-oxoethyl)<<(2,4-dioxo-1-imidazolidinyl)imino>methyl>formamide

There total 3 articles about N-(2-phenyl-2-oxoethyl)<<(2,4-dioxo-1-imidazolidinyl)imino>methyl>formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

2-aminoacetophenone hydrochloride (5468-37-1) + <<(2,4-dioxo-1-imidazolidinyl)imino>methyl>formic acid chloride (64748-90-9) → N-(2-phenyl-2-oxoethyl)<<(2,4-dioxo-1-imidazolidinyl)imino>methyl>formamide (64748-75-0)

Guidance literature:

With pyridine; In N,N-dimethyl-formamide;

DOI:10.1021/jm00385a006

Reference yield:

<<(2,4-dioxo-1-imidazolidinyl)imino>methyl>formic acid (64748-89-6) → N-(2-phenyl-2-oxoethyl)<<(2,4-dioxo-1-imidazolidinyl)imino>methyl>formamide (64748-75-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / SOCl₂ / dioxane / 5 h / Heating

2: 55 percent / pyridine / dimethylformamide

With pyridine; thionyl chloride; In 1,4-dioxane; N,N-dimethyl-formamide;

DOI:10.1021/jm00385a006

Reference yield:

→ N-(2-phenyl-2-oxoethyl)<<(2,4-dioxo-1-imidazolidinyl)imino>methyl>formamide (64748-75-0)

Guidance literature:

aus α-Aminoacetophenon m. entspr. Saeurechlorid;

upstream raw materials:

2-aminoacetophenone hydrochloride

<<(2,4-dioxo-1-imidazolidinyl)imino>methyl>formic acid chloride

<<(2,4-dioxo-1-imidazolidinyl)imino>methyl>formic acid

Downstream raw materials:

1-<<(5-phenyl-2-oxazolyl)methylene>amino>-2,4-imidazolidinedione

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