Technology Process of C27H36ClN5O7S
There total 8 articles about C27H36ClN5O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
tetrahydrofuran; methanol;
for 86h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: acetonitrile / 3 h / 80 °C
2: hydrogenchloride / methanol / 2 h
3: triethylamine / dichloromethane
4: dmap; triethylamine / tetrahydrofuran / 6 h / Reflux; Sealed tube
5: palladium on activated charcoal; hydrogen / tetrahydrofuran; methanol / 86 h
With
hydrogenchloride; dmap; palladium on activated charcoal; hydrogen; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: N-ethyl-N,N-diisopropylamine / acetonitrile / Reflux
2: dmap; triethylamine / tetrahydrofuran / 2 h / Reflux
3: potassium phosphate; tetrakis(triphenylphosphine) palladium(0); XPhos / 1,4-dioxane; water / 2 h / 80 °C / Inert atmosphere
4: acetonitrile / 3 h / 80 °C
5: hydrogenchloride / methanol / 2 h
6: triethylamine / dichloromethane
7: dmap; triethylamine / tetrahydrofuran / 6 h / Reflux; Sealed tube
8: palladium on activated charcoal; hydrogen / tetrahydrofuran; methanol / 86 h
With
hydrogenchloride; dmap; potassium phosphate; tetrakis(triphenylphosphine) palladium(0); palladium on activated charcoal; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; XPhos;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetonitrile;
3: |Suzuki Coupling;
