C₄₇H₈₆O₇Si₂

Base Information

Chemical Name:C₄₇H₈₆O₇Si₂
CAS No.:1448230-67-8
Molecular Formula:C₄₇H₈₆O₇Si₂
Molecular Weight:819.367
Hs Code.:

C<sub>47</sub>H<sub>86</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:C₄₇H₈₆O₇Si₂

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Chemical Property of C₄₇H₈₆O₇Si₂

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Technology Process of C₄₇H₈₆O₇Si₂

There total 5 articles about C₄₇H₈₆O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1279699-60-3
C₂₇H₂₉O₇P

: 1448230-65-6
C₃₂H₆₇IO₄Si₂

: 1448230-67-8
C₄₇H₈₆O₇Si₂

Guidance literature:: C₃₂H₆₇IO₄Si₂; With tert.-butyl lithium; 9-methoxy-9-BBN; In tetrahydrofuran; diethyl ether; hexane; pentane; at -78 - 20 ℃; for 4h;

With caesium carbonate; In tetrahydrofuran; diethyl ether; hexane; water; pentane; at 20 ℃; for 0.333333h;

C₂₇H₂₉O₇P; With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; diethyl ether; hexane; water; N,N-dimethyl-formamide; pentane; at 50 ℃; for 13h;
DOI:10.1021/ol4017518

Reference yield:

: C₂₂H₃₄O₄

: 1448230-67-8
C₄₇H₈₆O₇Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III); osmium(VIII) oxide; methanesulfonamide; potassium carbonate / water; tert-butyl alcohol / 23 h / 0 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1.17 h / 20 °C / pH 7

4.1: triethylamine; dmap / dichloromethane / 25 h / 0 - 20 °C

5.1: sodium iodide / acetone / 18 h / 50 °C

6.1: 9-methoxy-9-BBN; tert.-butyl lithium / tetrahydrofuran; hexane; diethyl ether; pentane / 4 h / -78 - 20 °C

6.2: 0.33 h / 20 °C

6.3: 13 h / 50 °C

With 2,6-dimethylpyridine; dmap; osmium(VIII) oxide; methanesulfonamide; tert.-butyl lithium; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; 9-methoxy-9-BBN; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; potassium hexacyanoferrate(III); In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; acetone; tert-butyl alcohol; pentane; 1.1: |Sharpless Dihydroxylation;
DOI:10.1021/ol4017518

Reference yield:

: 1448230-61-2
C₂₂H₃₆O₆

: 1448230-67-8
C₄₇H₈₆O₇Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1.17 h / 20 °C / pH 7

3.1: triethylamine; dmap / dichloromethane / 25 h / 0 - 20 °C

4.1: sodium iodide / acetone / 18 h / 50 °C

5.1: 9-methoxy-9-BBN; tert.-butyl lithium / tetrahydrofuran; hexane; diethyl ether; pentane / 4 h / -78 - 20 °C

5.2: 0.33 h / 20 °C

5.3: 13 h / 50 °C

With 2,6-dimethylpyridine; dmap; tert.-butyl lithium; triethylamine; 9-methoxy-9-BBN; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; acetone; pentane;
DOI:10.1021/ol4017518