methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-2-oxobutanoate

Base Information

Chemical Name:methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-2-oxobutanoate
CAS No.:1455092-81-5
Molecular Formula:C₂₂H₁₇N₃O₆
Molecular Weight:419.393
Hs Code.:

Synonyms:methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-2-oxobutanoate

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Chemical Property of methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-2-oxobutanoate

Chemical Property:

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Technology Process of methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-2-oxobutanoate

There total 3 articles about methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-2-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1455129-05-1
(S)-methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-2-hydroxybutanoate

: 1455092-81-5
methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-2-oxobutanoate

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 1455088-71-7
(S)-4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-2-hydroxybutanoic acid

: 1455092-81-5
methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-2-oxobutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 20 °C

2: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

With thionyl chloride; Dess-Martin periodane; In dichloromethane;

Reference yield:

: 1455091-23-2
1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxylic acid methyl ester

: 1455092-81-5
methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-2-oxobutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate / methanol / 1 h / 120 °C

2: thionyl chloride / 20 °C

3: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

With thionyl chloride; sodium methylate; Dess-Martin periodane; In methanol; dichloromethane;