1-(4-methoxybenzyl)-4-(5-amino-1-benzyl-1H-imidazol-4-yl)-5-imino-1H-imidazol-2(5H)-one

Base Information

• Chemical Name: 1-(4-methoxybenzyl)-4-(5-amino-1-benzyl-1H-imidazol-4-yl)-5-imino-1H-imidazol-2(5H)-one
• CAS No.: 1421053-58-8
• Molecular Formula: C₂₁H₂₀N₆O₂
• Molecular Weight: 388.429

Synonyms:1-(4-methoxybenzyl)-4-(5-amino-1-benzyl-1H-imidazol-4-yl)-5-imino-1H-imidazol-2(5H)-one

Chemical Property of 1-(4-methoxybenzyl)-4-(5-amino-1-benzyl-1H-imidazol-4-yl)-5-imino-1H-imidazol-2(5H)-one

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Technology Process of 1-(4-methoxybenzyl)-4-(5-amino-1-benzyl-1H-imidazol-4-yl)-5-imino-1H-imidazol-2(5H)-one

There total 2 articles about 1-(4-methoxybenzyl)-4-(5-amino-1-benzyl-1H-imidazol-4-yl)-5-imino-1H-imidazol-2(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C21H20N6O2 → 1-(4-methoxybenzyl)-4-(5-amino-1-benzyl-1H-imidazol-4-yl)-5-imino-1H-imidazol-2(5H)-one (1421053-58-8)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 3h;

DOI:10.1016/j.bmc.2012.11.050

Reference yield:

2-(5-amino-1-benzyl-1H-imidazol-4-yl)-2-iminoacetonitrile (156273-72-2) → 1-(4-methoxybenzyl)-4-(5-amino-1-benzyl-1H-imidazol-4-yl)-5-imino-1H-imidazol-2(5H)-one (1421053-58-8)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 12 h / 20 °C / Inert atmosphere

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 3 h / 20 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile;

DOI:10.1016/j.bmc.2012.11.050

Reference yield:

1-(4-methoxybenzyl)-4-(5-amino-1-benzyl-1H-imidazol-4-yl)-5-imino-1H-imidazol-2(5H)-one (1421053-58-8) + orthoformic acid triethyl ester (122-51-0) → C22H18N6O2 (1421053-61-3)

Guidance literature:

With sulfuric acid; for 2h; Inert atmosphere; Reflux;

DOI:10.1016/j.bmc.2012.11.050

upstream raw materials:

2-(5-amino-1-benzyl-1H-imidazol-4-yl)-2-iminoacetonitrile

Downstream raw materials:

C₂₂H₁₈N₆O₂

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