toluene-4-sulfonic acid 5-(4'-chloro-biphenyl-4-yloxy)-3-methyl-pentyl ester

Base Information

Chemical Name:toluene-4-sulfonic acid 5-(4'-chloro-biphenyl-4-yloxy)-3-methyl-pentyl ester
CAS No.:866750-97-2
Molecular Formula:C₂₅H₂₇ClO₄S
Molecular Weight:459.006
Hs Code.:

Synonyms:toluene-4-sulfonic acid 5-(4'-chloro-biphenyl-4-yloxy)-3-methyl-pentyl ester

Suppliers and Price of toluene-4-sulfonic acid 5-(4'-chloro-biphenyl-4-yloxy)-3-methyl-pentyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of toluene-4-sulfonic acid 5-(4'-chloro-biphenyl-4-yloxy)-3-methyl-pentyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of toluene-4-sulfonic acid 5-(4'-chloro-biphenyl-4-yloxy)-3-methyl-pentyl ester

There total 5 articles about toluene-4-sulfonic acid 5-(4'-chloro-biphenyl-4-yloxy)-3-methyl-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 148054-23-3
3-methylpentane-1,5-diyl bis(4-methylbenzenesulfonate)

: 28034-99-3
4'-Chloro-4-biphenylol

: 866750-97-2
toluene-4-sulfonic acid 5-(4'-chloro-biphenyl-4-yloxy)-3-methyl-pentyl ester

Guidance literature:: With potassium carbonate; In acetonitrile; at 60 ℃; for 24h;
DOI:10.1021/jm050033v

Reference yield:

: 5164-76-1
dimethyl glutaconate

: 866750-97-2
toluene-4-sulfonic acid 5-(4'-chloro-biphenyl-4-yloxy)-3-methyl-pentyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: CuI / tetrahydrofuran / 20 °C

1.2: TMSCl / tetrahydrofuran / -78 - 20 °C

2.1: lithium aluminum hydride / tetrahydrofuran / 24 h / Heating

3.1: pyridine / 2 h / 20 °C

4.1: K₂CO₃ / acetonitrile / 24 h / 60 °C

With pyridine; copper(l) iodide; lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetonitrile; 1.2: Michael addition;
DOI:10.1021/jm050033v

Reference yield:

: 4457-71-0
3-methylpentane-1,5-diol

: 866750-97-2
toluene-4-sulfonic acid 5-(4'-chloro-biphenyl-4-yloxy)-3-methyl-pentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1 h / 20 °C

2: K₂CO₃ / acetonitrile / Heating

With pyridine; potassium carbonate; In acetonitrile;
DOI:10.1016/j.bmcl.2005.06.069