geranyl 2,3,4,2',3',4'-O-hexabenzoyl-β-D-xylopyranosyl-(1->6)-β-D-glucopyranoside

Base Information

Chemical Name:geranyl 2,3,4,2',3',4'-O-hexabenzoyl-β-D-xylopyranosyl-(1->6)-β-D-glucopyranoside
CAS No.:192827-14-8
Molecular Formula:C₆₃H₆₀O₁₆
Molecular Weight:1073.16
Hs Code.:

Synonyms:geranyl 2,3,4,2',3',4'-O-hexabenzoyl-β-D-xylopyranosyl-(1->6)-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of geranyl 2,3,4,2',3',4'-O-hexabenzoyl-β-D-xylopyranosyl-(1->6)-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of geranyl 2,3,4,2',3',4'-O-hexabenzoyl-β-D-xylopyranosyl-(1->6)-β-D-glucopyranoside

There total 10 articles about geranyl 2,3,4,2',3',4'-O-hexabenzoyl-β-D-xylopyranosyl-(1->6)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 192827-18-2
geranyl 2,3,4-tri-O-benzoyl-β-D-glucopyranoside

: 14262-83-0
2,3,4-tri-O-benzoyl-α-D-xylopyranosyl bromide

: 192827-14-8
geranyl 2,3,4,2',3',4'-O-hexabenzoyl-β-D-xylopyranosyl-(1->6)-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; tetramethylurea; In dichloromethane; at 20 ℃; for 18h;
DOI:10.3987/COM-05-10640

Reference yield:

: 104707-01-9
1,2,3,4-tetra-O-benzoyl-β-D-glucopyranose

: 192827-14-8
geranyl 2,3,4,2',3',4'-O-hexabenzoyl-β-D-xylopyranosyl-(1->6)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: Hg(CN)2 / acetonitrile / 3 h / Ambient temperature

2: 33.3 percent / TiBr₄ / CH₂Cl₂; ethyl acetate / 1 h / Ambient temperature

3: Hg(CN)2 / acetonitrile / 3 h / Ambient temperature

With mercury(II) cyanide; titanium(IV) bromide; In dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1021/jf960852b

Reference yield:

: 192827-10-4
2,3,4-tri-O-benzoyl-β-D-xylopyranosyl-(1->6)-1,2,3,4-tera-O-benzoyl-β-D-glucopyranose

: 192827-14-8
geranyl 2,3,4,2',3',4'-O-hexabenzoyl-β-D-xylopyranosyl-(1->6)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 33.3 percent / TiBr₄ / CH₂Cl₂; ethyl acetate / 1 h / Ambient temperature

2: Hg(CN)2 / acetonitrile / 3 h / Ambient temperature

With mercury(II) cyanide; titanium(IV) bromide; In dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1021/jf960852b