N,N'-bis-(2-benzylthio-2-methylpropyl)-2-(benzylthiomethyl)-2-methylmalonyl diamide

Base Information

Chemical Name:N,N'-bis-(2-benzylthio-2-methylpropyl)-2-(benzylthiomethyl)-2-methylmalonyl diamide
CAS No.:256505-80-3
Molecular Formula:C₃₄H₄₄N₂O₂S₃
Molecular Weight:608.934
Hs Code.:

Synonyms:N,N'-bis-(2-benzylthio-2-methylpropyl)-2-(benzylthiomethyl)-2-methylmalonyl diamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis-(2-benzylthio-2-methylpropyl)-2-(benzylthiomethyl)-2-methylmalonyl diamide

Chemical Property:

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Technology Process of N,N'-bis-(2-benzylthio-2-methylpropyl)-2-(benzylthiomethyl)-2-methylmalonyl diamide

There total 3 articles about N,N'-bis-(2-benzylthio-2-methylpropyl)-2-(benzylthiomethyl)-2-methylmalonyl diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 59681-09-3
2-benzylthio 2-methyl propylamine

: 256505-79-0
diethyl 2-(benzylthiomethyl)-2-methylmalonate

: 256505-80-3
N,N'-bis-(2-benzylthio-2-methylpropyl)-2-(benzylthiomethyl)-2-methylmalonyl diamide

Guidance literature:: 2-benzylthio 2-methyl propylamine; With trimethylaluminum; In dichloromethane; at -15 - 25 ℃;

diethyl 2-(benzylthiomethyl)-2-methylmalonate; In dichloromethane; at 40 ℃; for 48h;
DOI:10.1081/SCC-100104041

Reference yield:

: 3970-13-6
benzyl chloromethyl sulfide

: 256505-80-3
N,N'-bis-(2-benzylthio-2-methylpropyl)-2-(benzylthiomethyl)-2-methylmalonyl diamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 75 percent / NaH / dimethylformamide / -10 - 25 °C

2.1: AlMe₃ / CH₂Cl₂ / -15 - 25 °C

2.2: 80 percent / CH₂Cl₂ / 48 h / 40 °C

With trimethylaluminum; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/SCC-100104041

Reference yield:

: 100-53-8
phenylmethanethiol

: 256505-80-3
N,N'-bis-(2-benzylthio-2-methylpropyl)-2-(benzylthiomethyl)-2-methylmalonyl diamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 100 percent / potassium hydroxide; triethylbenzylammonium chloride / 1 h / 20 °C

2.1: 75 percent / NaH / dimethylformamide / -10 - 25 °C

3.1: AlMe₃ / CH₂Cl₂ / -15 - 25 °C

3.2: 80 percent / CH₂Cl₂ / 48 h / 40 °C

With potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; trimethylaluminum; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/SCC-100104041