methyl 4-[6-(4-bromophenyl)-3-oxo-4,5-dihydro-2H-pyridazin-4-ylmethyl]benzoate

Base Information

Chemical Name:methyl 4-[6-(4-bromophenyl)-3-oxo-4,5-dihydro-2H-pyridazin-4-ylmethyl]benzoate
CAS No.:692754-52-2
Molecular Formula:C₁₉H₁₇BrN₂O₃
Molecular Weight:401.26
Hs Code.:

Synonyms:methyl 4-[6-(4-bromophenyl)-3-oxo-4,5-dihydro-2H-pyridazin-4-ylmethyl]benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-[6-(4-bromophenyl)-3-oxo-4,5-dihydro-2H-pyridazin-4-ylmethyl]benzoate

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Technology Process of methyl 4-[6-(4-bromophenyl)-3-oxo-4,5-dihydro-2H-pyridazin-4-ylmethyl]benzoate

There total 4 articles about methyl 4-[6-(4-bromophenyl)-3-oxo-4,5-dihydro-2H-pyridazin-4-ylmethyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 692754-50-0
methyl 4-{5-[2-(4-bromophenyl)-2-oxoethyl]-2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylmethyl}benzoate

: 692754-52-2
methyl 4-[6-(4-bromophenyl)-3-oxo-4,5-dihydro-2H-pyridazin-4-ylmethyl]benzoate

Guidance literature:: With hydrazine hydrate; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1081/SCC-120028351

Reference yield:

: 619-66-9
4-Carboxybenzaldehyde

: 692754-52-2
methyl 4-[6-(4-bromophenyl)-3-oxo-4,5-dihydro-2H-pyridazin-4-ylmethyl]benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 1 h / 20 °C

2: 73 percent / triethylammonium formate / 72 h / 20 °C

3: 73 percent / sodium acetate; acetic acid / dimethylformamide / 20 °C

4: 75 percent / hydrazine monohydrate / dimethylformamide / 0 - 20 °C

With sodium acetate; triethylammonium formate; hydrazine hydrate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1081/SCC-120028351

Reference yield:

: 1571-08-0
methyl 4-formylbenzoate

: 692754-52-2
methyl 4-[6-(4-bromophenyl)-3-oxo-4,5-dihydro-2H-pyridazin-4-ylmethyl]benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / triethylammonium formate / 72 h / 20 °C

2: 73 percent / sodium acetate; acetic acid / dimethylformamide / 20 °C

3: 75 percent / hydrazine monohydrate / dimethylformamide / 0 - 20 °C

With sodium acetate; triethylammonium formate; hydrazine hydrate; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1081/SCC-120028351