Technology Process of C32H42FN3O7
There total 13 articles about C32H42FN3O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium acetate; caesium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 40 °C
2.1: hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 0.08 h / 20 °C
3.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 3 h / pH 2
4.1: toluene / Heating / reflux
5.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C
6.1: trimethylaluminum / hexanes; dichloromethane / 0.25 h
6.2: 20 °C
7.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide
With
hydrogenchloride; hydroxylamine hydrochloride; methyl orange; trimethylaluminum; potassium acetate; sodium cyanoborohydride; potassium carbonate; caesium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran; methanol; hexanes; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 0.08 h / 20 °C
2.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 3 h / pH 2
3.1: toluene / Heating / reflux
4.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C
5.1: trimethylaluminum / hexanes; dichloromethane / 0.25 h
5.2: 20 °C
6.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide
With
hydrogenchloride; hydroxylamine hydrochloride; methyl orange; trimethylaluminum; potassium acetate; sodium cyanoborohydride; caesium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran; methanol; hexanes; dichloromethane; water; dimethyl sulfoxide; toluene;