(+/-)-1-(3-benzyloxy-4,5-dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)butan-1,4-diol

Base Information

Chemical Name:(+/-)-1-(3-benzyloxy-4,5-dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)butan-1,4-diol
CAS No.:180900-47-4
Molecular Formula:C₂₈H₃₄O₈
Molecular Weight:498.573
Hs Code.:

Synonyms:(+/-)-1-(3-benzyloxy-4,5-dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)butan-1,4-diol

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Chemical Property of (+/-)-1-(3-benzyloxy-4,5-dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)butan-1,4-diol

Chemical Property:

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Technology Process of (+/-)-1-(3-benzyloxy-4,5-dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)butan-1,4-diol

There total 1 articles about (+/-)-1-(3-benzyloxy-4,5-dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)butan-1,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 180900-31-6
1-(3-benzyloxy-4,5-dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)butan-1,4-dione

: 180900-47-4
(+/-)-1-(3-benzyloxy-4,5-dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)butan-1,4-diol

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 70 ℃; for 1.33333h;
DOI:10.1016/0223-5234(96)89161-6

Reference yield:

: 180900-47-4
(+/-)-1-(3-benzyloxy-4,5-dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)butan-1,4-diol

: 2,3-Dimethoxy-5-[(2S,5S)-5-(3,4,5-trimethoxy-phenyl)-tetrahydro-furan-2-yl]-phenol

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / CHCl₃ / 1.33 h / Ambient temperature

2: 94 percent / H₂ / 5percent Pd/C / ethanol / 760 Torr / Ambient temperature

With hydrogen; trifluoroacetic acid; palladium on activated charcoal; In ethanol; chloroform;
DOI:10.1016/0223-5234(96)89161-6

Reference yield:

: 180900-47-4
(+/-)-1-(3-benzyloxy-4,5-dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)butan-1,4-diol

: 2,3-Dimethoxy-5-[(2R,5S)-5-(3,4,5-trimethoxy-phenyl)-tetrahydro-furan-2-yl]-phenol

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / CHCl₃ / 1.33 h / Ambient temperature

2: 75 percent / H₂ / 5percent Pd/C / ethanol / 760 Torr / Ambient temperature

With hydrogen; trifluoroacetic acid; palladium on activated charcoal; In ethanol; chloroform;
DOI:10.1016/0223-5234(96)89161-6