4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid

Base Information

Chemical Name:4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid
CAS No.:108826-77-3
Molecular Formula:C₆₅H₈₆IN₁₁O₁₃
Molecular Weight:1356.37
Hs Code.:

4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid

Synonyms:4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid

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Chemical Property of 4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid

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Technology Process of 4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid

There total 1 articles about 4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 108826-76-2
4-butanoic acid

: 108826-77-3
4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid

Guidance literature:: With acetic acid; at 50 ℃; for 1h;

Reference yield: 31.0%

: 108826-77-3
4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid

: 108826-78-4
cyclo-<4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid>

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 50 ℃; for 20h;

Reference yield:

: 108826-77-3
4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid

: 108827-34-5
cyclo-<4-(asparaginyl-<4-(3)H>phenylalanyl-D-tryptophyl-lysylthreonylphenylalanylamino)butanoic acid>

Guidance literature:: Multi-step reaction with 3 steps

1: 31 percent / DCC, HOBt / dimethylformamide / 20 h / 50 °C

2: tritium / 10percent Pd-C, 5percent Rh-CaCO₃ / dimethylformamide / 0.67 h / Ambient temperature

3: 90percent aq. CF₃COOH / 1 h / Ambient temperature

With tritium; benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; palladium on activated charcoal; rhodium on CaCO₃; In N,N-dimethyl-formamide;