Technology Process of bis(phenylphosphine)(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)iron(II)
There total 1 articles about bis(phenylphosphine)(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)iron(II) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
NaS2O4;
In
dichloromethane; water;
under N2; soln. of Na2S2O4 in H2O mixed with soln. of Fe compd. in CH2Cl2; stirred for 15 min; phosphine (excess) added; stirred for 5 min; org. phase sepd.; dried (anhyd. Na2SO4); evapd. to dryness in vac.; washed with hexane; elem. anal.;
DOI:10.1021/ic800484k