(S)-(+)-N-<5-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-cyanessigsaeureamid

Base Information

Chemical Name:(S)-(+)-N-<5-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-cyanessigsaeureamid
CAS No.:154334-40-4
Molecular Formula:C₁₃H₁₄ClN₃O₃
Molecular Weight:295.725
Hs Code.:

Synonyms:(S)-(+)-N-<5-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-cyanessigsaeureamid

Suppliers and Price of (S)-(+)-N-<5-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-cyanessigsaeureamid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(+)-N-<5-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-cyanessigsaeureamid

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Technology Process of (S)-(+)-N-<5-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-cyanessigsaeureamid

There total 1 articles about (S)-(+)-N-<5-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-cyanessigsaeureamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 35966-84-8
4-chloro-2-methylaminonitrobenzene

: (S)-(-)-Ethylmethylcyanessigsaeurechlorid

: 154334-40-4
(S)-(+)-N-<5-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-cyanessigsaeureamid

Guidance literature:: In pyridine; Heating;
DOI:10.1002/ardp.19933260911

Reference yield: 89.0%

: 154334-40-4
(S)-(+)-N-<5-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-cyanessigsaeureamid

: 154003-68-6
(S)-(+)-N-<5-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-malonsaeurediamid

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; In methanol;
DOI:10.1002/ardp.19933260911

Reference yield:

: 154334-40-4
(S)-(+)-N-<5-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-cyanessigsaeureamid

: (R)-(-)-8-Chlor-3-ethyl-1,3-dimethyl-5-phenyl-1H-1,5-benzodiazepin(3H,5H)-2,4-dion

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / 30percent H₂O₂, 0.5N NaOH / methanol

2: 49 percent / Zn-powder / aq. HCl / 24 h / Ambient temperature

3: 95 percent / kaliumacetate, Cu-powder / 6.5 h / 150 °C

With sodium hydroxide; dihydrogen peroxide; potassium acetate; copper; zinc; In hydrogenchloride; methanol;
DOI:10.1002/ardp.19933260911