diethyl acetonyl>amino>benzoyl>-L-glutamate

Base Information

Chemical Name:diethyl acetonyl>amino>benzoyl>-L-glutamate
CAS No.:101760-55-8
Molecular Formula:2C₂₆H₃₁N₇O₉*ClH
Molecular Weight:1207.61
Hs Code.:

diethyl <p-<N-propargyl-N-<3-<(2-amino-4-hydroxy-5-nitropyrimidin-6-yl)amino>acetonyl>amino>benzoyl>-L-glutamate

Synonyms:diethyl acetonyl>amino>benzoyl>-L-glutamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl acetonyl>amino>benzoyl>-L-glutamate

Chemical Property:

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Technology Process of diethyl acetonyl>amino>benzoyl>-L-glutamate

There total 3 articles about diethyl acetonyl>amino>benzoyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 101760-53-6
diethyl acetonyl>amino>benzoyl>-L-glutamate oxime

: 101760-55-8
diethyl acetonyl>amino>benzoyl>-L-glutamate

Guidance literature:: With hydrogenchloride; In trifluoroacetic acid; at 60 - 65 ℃;
DOI:10.1021/jm00157a600

Reference yield:

: 101760-51-4,101760-59-2
diethyl benzoyl>-L-glutamate oxime

: 101760-55-8
diethyl acetonyl>amino>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / 4-methylmorpholine / methanol / 4 h / Heating

2: 100 percent / 0.1 N HCl / trifluoroacetic acid / 60 - 65 °C

With 4-methyl-morpholine; hydrogenchloride; In methanol; trifluoroacetic acid;
DOI:10.1021/jm00157a600

Reference yield:

: 101760-49-0,101760-58-1
diethyl benzoyl>-L-glutamate oxime

: 101760-55-8
diethyl acetonyl>amino>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / hydrazine / methanol / 72 h

2: 68 percent / 4-methylmorpholine / methanol / 4 h / Heating

3: 100 percent / 0.1 N HCl / trifluoroacetic acid / 60 - 65 °C

With 4-methyl-morpholine; hydrogenchloride; hydrazine; In methanol; trifluoroacetic acid;
DOI:10.1021/jm00157a600