5-methyl-1-hexyl tosylate

Base Information

• Chemical Name: 5-methyl-1-hexyl tosylate
• CAS No.: 951405-21-3
• Molecular Formula: C₁₄H₂₂O₃S
• Molecular Weight: 270.393
• Mol file: 951405-21-3.mol

Synonyms:5-methyl-1-hexyl tosylate

Chemical Property of 5-methyl-1-hexyl tosylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 5-methyl-1-hexyl tosylate

There total 2 articles about 5-methyl-1-hexyl tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

5-methyl-1-hexanol (627-98-5) + p-toluenesulfonyl chloride (98-59-9) → 5-methyl-1-hexyl tosylate (951405-21-3)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 ℃;

Reference yield:

5-methylhexanoic acid (628-46-6) → 5-methyl-1-hexyl tosylate (951405-21-3)

Guidance literature:

Multi-step reaction with 2 steps

1: dimethylsulfide borane complex / tetrahydrofuran / 12 h / 20 °C

2: triethylamine; dmap / dichloromethane / 0.5 h / 20 °C

With dmap; dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield: 55.0%

5-methyl-1-hexyl tosylate (951405-21-3) → 5-methylhexyl bromide (35354-37-1)

Guidance literature:

With lithium bromide; In N,N-dimethyl-formamide; at 45 ℃; for 3h;

upstream raw materials:

5-methyl-1-hexanol

p-toluenesulfonyl chloride

5-methylhexanoic acid

Downstream raw materials:

5-methylhexyl bromide

isononoic acid