(S)-2-(5-methoxybenzofuran-2-carboxamido)-3-(2-methylbenzyloxy)propanoic acid

Base Information

Chemical Name:(S)-2-(5-methoxybenzofuran-2-carboxamido)-3-(2-methylbenzyloxy)propanoic acid
CAS No.:1352825-54-7
Molecular Formula:C₂₁H₂₁NO₆
Molecular Weight:383.401
Hs Code.:

Synonyms:(S)-2-(5-methoxybenzofuran-2-carboxamido)-3-(2-methylbenzyloxy)propanoic acid

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Chemical Property of (S)-2-(5-methoxybenzofuran-2-carboxamido)-3-(2-methylbenzyloxy)propanoic acid

Chemical Property:

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Technology Process of (S)-2-(5-methoxybenzofuran-2-carboxamido)-3-(2-methylbenzyloxy)propanoic acid

There total 5 articles about (S)-2-(5-methoxybenzofuran-2-carboxamido)-3-(2-methylbenzyloxy)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₃NO₆

: 1352825-54-7
(S)-2-(5-methoxybenzofuran-2-carboxamido)-3-(2-methylbenzyloxy)propanoic acid

Guidance literature:: C₂₂H₂₃NO₆; With ethanol; sodium hydroxide; at 20 ℃; for 4h;

With hydrogenchloride; In water;

Reference yield:

: 89-92-9
2-methylbenzyl bromide

: 1352825-54-7
(S)-2-(5-methoxybenzofuran-2-carboxamido)-3-(2-methylbenzyloxy)propanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / dichloromethane; water / 18 h / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

3: triethylamine / dichloromethane / 2 h / 20 °C

4: sodium hydroxide; ethanol / 4 h / 20 °C

With ethanol; N-benzyl-N,N,N-triethylammonium chloride; triethylamine; trifluoroacetic acid; sodium hydroxide; In dichloromethane; water;

Reference yield:

: 10242-08-7
5-methoxybenzofuran-2-carboxylic acid

: 1352825-54-7
(S)-2-(5-methoxybenzofuran-2-carboxamido)-3-(2-methylbenzyloxy)propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / Reflux

2: triethylamine / dichloromethane / 2 h / 20 °C

3: sodium hydroxide; ethanol / 4 h / 20 °C

With thionyl chloride; ethanol; triethylamine; sodium hydroxide; In dichloromethane;