C₆₁H₇₅FO₁₂SSi

Base Information

Chemical Name:C₆₁H₇₅FO₁₂SSi
CAS No.:1373634-66-2
Molecular Formula:C₆₁H₇₅FO₁₂SSi
Molecular Weight:1079.41
Hs Code.:

C<sub>61</sub>H<sub>75</sub>FO<sub>12</sub>SSi

Synonyms:C₆₁H₇₅FO₁₂SSi

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Chemical Property of C₆₁H₇₅FO₁₂SSi

Chemical Property:

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Technology Process of C₆₁H₇₅FO₁₂SSi

There total 8 articles about C₆₁H₇₅FO₁₂SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1373634-63-9
C₃₀H₄₃IO₃Si

: 1373634-60-6
C₃₁H₃₁FO₉S

: 1373634-66-2
C₆₁H₇₅FO₁₂SSi

Guidance literature:: With chromium dichloride; manganese; zirconocene dichloride; N-(2-((S)-4-isopropyl-4,5-dihydrooxazol-2-yl)-6-(((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl)oxy)phenyl)benzenesulfonamide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; lithium chloride; In acetonitrile; at 20 ℃; for 4h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol300672q

Reference yield:

: 1191256-12-8
C₂₅H₂₆O₇

: 1373634-66-2
C₆₁H₇₅FO₁₂SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran; toluene / 0.17 h / 0 - 20 °C / Inert atmosphere

1.2: 0.67 h / 20 °C / Inert atmosphere

2.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

3.1: sodium periodate; sodium hydrogencarbonate / dichloromethane; water / 20 °C / Inert atmosphere

4.1: sodium tetrahydroborate / methanol / 0.17 h / 0 °C / Inert atmosphere

5.1: Crabtree's catalyst; hydrogen / dichloromethane / 0 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere

7.1: chromium dichloride; manganese; zirconocene dichloride; N-(2-((S)-4-isopropyl-4,5-dihydrooxazol-2-yl)-6-(((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl)oxy)phenyl)benzenesulfonamide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; lithium chloride / acetonitrile / 4 h / 20 °C / Inert atmosphere

With chromium dichloride; manganese; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; zirconocene dichloride; Crabtree's catalyst; N-(2-((S)-4-isopropyl-4,5-dihydrooxazol-2-yl)-6-(((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl)oxy)phenyl)benzenesulfonamide; water; hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; sodium hydrogencarbonate; Dess-Martin periodane; 4-methylmorpholine N-oxide; lithium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/ol300672q

Reference yield:

: 1373634-51-5
C₃₂H₃₁FO₈S

: 1373634-66-2
C₆₁H₇₅FO₁₂SSi

Guidance literature:: Multi-step reaction with 6 steps

1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

2: sodium periodate; sodium hydrogencarbonate / dichloromethane; water / 20 °C / Inert atmosphere

3: sodium tetrahydroborate / methanol / 0.17 h / 0 °C / Inert atmosphere

4: Crabtree's catalyst; hydrogen / dichloromethane / 0 °C / Inert atmosphere

5: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere

6: chromium dichloride; manganese; zirconocene dichloride; N-(2-((S)-4-isopropyl-4,5-dihydrooxazol-2-yl)-6-(((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl)oxy)phenyl)benzenesulfonamide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; lithium chloride / acetonitrile / 4 h / 20 °C / Inert atmosphere

With chromium dichloride; manganese; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; zirconocene dichloride; Crabtree's catalyst; N-(2-((S)-4-isopropyl-4,5-dihydrooxazol-2-yl)-6-(((1S,2R,5S)-2-isopropyl-5-methylcyclohexyl)oxy)phenyl)benzenesulfonamide; water; hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; sodium hydrogencarbonate; Dess-Martin periodane; 4-methylmorpholine N-oxide; lithium chloride; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ol300672q