(S)-tert-butyl 4-hydroxy-4-phenylbutanoate

Base Information

Chemical Name:(S)-tert-butyl 4-hydroxy-4-phenylbutanoate
CAS No.:1006728-95-5
Molecular Formula:C₁₄H₂₀O₃
Molecular Weight:236.311
Hs Code.:

Synonyms:(S)-tert-butyl 4-hydroxy-4-phenylbutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-tert-butyl 4-hydroxy-4-phenylbutanoate

Chemical Property:

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Technology Process of (S)-tert-butyl 4-hydroxy-4-phenylbutanoate

There total 10 articles about (S)-tert-butyl 4-hydroxy-4-phenylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 55666-45-0
4-oxo-4-phenyl-butyric acid tert-butyl ester

: 1006728-95-5
(S)-tert-butyl 4-hydroxy-4-phenylbutanoate

Guidance literature:: With (-)-diisopinocamphenylborane chloride; In tetrahydrofuran; at -78 - 20 ℃; for 12h;
DOI:10.1021/ja0772750

Reference yield:

: 55666-45-0
4-oxo-4-phenyl-butyric acid tert-butyl ester

: 1006728-95-5
(S)-tert-butyl 4-hydroxy-4-phenylbutanoate

: tert-butyl 4-hydroxy-4-phenylbutanoate

Guidance literature:: With D-glucose; In aq. phosphate buffer; at 28 ℃; for 18h; pH=7; Overall yield = 60 %; enantioselective reaction; Microbiological reaction;
DOI:10.1016/j.tetlet.2014.10.133

Reference yield:

: 55666-45-0
4-oxo-4-phenyl-butyric acid tert-butyl ester

: 1006728-95-5
(S)-tert-butyl 4-hydroxy-4-phenylbutanoate

: 111138-02-4
(-)-(S)-5-phenyl-4,5-dihydrofuran-2(3H)-one

Guidance literature:: With [RuBr₂{(S,S)-2,4-bis-[(3,5-diisopropylphenyl)phosphanyl]pentane}(3-aminomethylisoquinoline)]; potassium tert-butylate; hydrogen; In ethanol; at 25 ℃; for 2h; under 6080.41 Torr; enantioselective reaction; Autoclave;
DOI:10.1002/anie.201711363