N-(4-phenylbutyl)fluorenimine

Base Information

• Chemical Name: N-(4-phenylbutyl)fluorenimine
• CAS No.: 119437-40-0
• Molecular Formula: C₂₃H₂₁N
• Molecular Weight: 311.426

Synonyms:N-(4-phenylbutyl)fluorenimine

Chemical Property of N-(4-phenylbutyl)fluorenimine

Chemical Property:

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Technology Process of N-(4-phenylbutyl)fluorenimine

There total 1 articles about N-(4-phenylbutyl)fluorenimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

9-fluorenone (486-25-9,952573-42-1) + 4-phenyl-1-butylamine (13214-66-9) → N-(4-phenylbutyl)fluorenimine (119437-40-0)

Guidance literature:

With titanium tetrachloride; In toluene; 1.) 25 deg C, 1 h, 2.) 100 to 110 deg C;

DOI:10.1021/jo00270a034

Reference yield:

n-butyllithium (109-72-8,29786-93-4) + N-(4-phenylbutyl)fluorenimine (119437-40-0) → (9-Butyl-9H-fluoren-9-yl)-(4-phenyl-butyl)-amine + N-butyl-N-(4-phenylbutyl)-9-aminofluorene (119437-43-3)

Guidance literature:

In tetrahydrofuran; hexane; 1.) -78 deg C, 2 h, 2.) 0 deg C, 10 min;

DOI:10.1021/jo00270a034

upstream raw materials:

9-fluorenone

4-phenyl-1-butylamine

Downstream raw materials:

N-butyl-N-(4-phenylbutyl)-9-aminofluorene

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