N'-[(E)-(2-methoxyphenyl)methylidene]benzenesulfonohydrazide

Base Information

• Chemical Name: N'-[(E)-(2-methoxyphenyl)methylidene]benzenesulfonohydrazide
• CAS No.: 145260-32-8
• Molecular Formula: C₁₄H₁₄N₂O₃S
• Molecular Weight: 290.343
• DSSTox Substance ID: DTXSID201332654
• ChEMBL ID: CHEMBL3214208
• Mol file: 145260-32-8.mol

Synonyms:145260-32-8;N'-[(E)-(2-methoxyphenyl)methylidene]benzenesulfonohydrazide;N'-[(1E)-(2-methoxyphenyl)methylidene]benzenesulfonohydrazide;N-[(E)-(2-methoxyphenyl)methylideneamino]benzenesulfonamide;(E)-N'-(2-methoxybenzylidene)benzenesulfonohydrazide;MLS001165992;CHEMBL3214208;DTXSID201332654;MFCD01225005;STK437758;AKOS003240055;SMR000550262;CS-0334062;AB00089926-01;3W-0634

Chemical Property of N'-[(E)-(2-methoxyphenyl)methylidene]benzenesulfonohydrazide

Chemical Property:

• XLogP3: 2.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 5
• Exact Mass: 290.07251349
• Heavy Atom Count: 20
• Complexity: 411

Purity/Quality:

99% ^*data from raw suppliers

N'-[(E)-(2-METHOXYPHENYL)METHYLIDENE]BENZENESULFONOHYDRAZIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC=CC=C1C=NNS(=O)(=O)C2=CC=CC=C2
• Isomeric SMILES: COC1=CC=CC=C1/C=N/NS(=O)(=O)C2=CC=CC=C2

Technology Process of N'-[(E)-(2-methoxyphenyl)methylidene]benzenesulfonohydrazide

There total 2 articles about N'-[(E)-(2-methoxyphenyl)methylidene]benzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

ortho-anisaldehyde (135-02-4) + benzenesufonyl hydrazide (80-17-1) → (E)-N'-(2-methoxybenzylidene)benzenesulfonohydrazide (145260-32-8)

Guidance literature:

In ethanol; at 20 ℃; for 1h;

DOI:10.1002/chem.201904138

Reference yield:

→ (E)-N'-(2-methoxybenzylidene)benzenesulfonohydrazide (145260-32-8)

Guidance literature:

/BRN= 3035007/;

Reference yield: 72.0%

C14H14N2O3S (145260-32-8) + 2-methoxybenzenediazonium chloride (3425-23-8) → 2,5-bis(2-methoxyphenyl)-2H-tetrazole (737733-33-4)

Guidance literature:

With pyridine; at -15 ℃;

DOI:10.1002/chem.201002360

upstream raw materials:

ortho-anisaldehyde

benzenesufonyl hydrazide

Downstream raw materials:

3-(1,3-bis(2-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)propan-1-ol

2,5-bis(o-phenolyl)tetrazole

2,5-bis(2-methoxyphenyl)-2H-tetrazole