C₃₉H₅₂O₃Si

Base Information

Chemical Name:C₃₉H₅₂O₃Si
CAS No.:932024-60-7
Molecular Formula:C₃₉H₅₂O₃Si
Molecular Weight:596.926
Hs Code.:

C<sub>39</sub>H<sub>52</sub>O<sub>3</sub>Si

Synonyms:C₃₉H₅₂O₃Si

Suppliers and Price of C₃₉H₅₂O₃Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₉H₅₂O₃Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₉H₅₂O₃Si

There total 7 articles about C₃₉H₅₂O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 932024-73-2
C₃₉H₅₀O₄Si

: 932024-60-7
C₃₉H₅₂O₃Si

Guidance literature:: C₃₉H₅₀O₄Si; With diisobutylaluminium hydride; In dichloromethane; at -78 ℃;

With carbon disulfide; potassium hydride; methyl iodide; In tetrahydrofuran; at 20 ℃;

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; Further stages.; Heating;
DOI:10.1016/j.tetlet.2007.01.024

Reference yield:

: 932024-62-9
C₂₇H₃₄O₂Si

: 932024-60-7
C₃₉H₅₂O₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: t-BuLi; lithium 2-thienylcyanocuprate / diethyl ether; tetrahydrofuran / -78 - -10 °C

1.2: 91 percent / diethyl ether; tetrahydrofuran / -78 - -30 °C

2.1: 99 percent / aq. TsOH / acetone / Heating

3.1: 82 percent / Cs₂CO₃ / acetonitrile / Heating

4.1: DIBAL-H / CH₂Cl₂ / -78 °C

4.2: KH; CS₂; MeI / tetrahydrofuran / 20 °C

4.3: n-Bu₃SnH; AIBN / benzene / Heating

With tert.-butyl lithium; diisobutylaluminium hydride; caesium carbonate; toluene-4-sulfonic acid; thien-2-yl(cyano)copper lithium; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; acetonitrile;
DOI:10.1016/j.tetlet.2007.01.024

Reference yield:

: 932024-66-3
C₂₇H₃₆OSi

: 932024-60-7
C₃₉H₅₂O₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 63 percent / K₂CO₃; org. peroxide / benzene / 20 °C

2.1: t-BuLi; lithium 2-thienylcyanocuprate / diethyl ether; tetrahydrofuran / -78 - -10 °C

2.2: 91 percent / diethyl ether; tetrahydrofuran / -78 - -30 °C

3.1: 99 percent / aq. TsOH / acetone / Heating

4.1: 82 percent / Cs₂CO₃ / acetonitrile / Heating

5.1: DIBAL-H / CH₂Cl₂ / -78 °C

5.2: KH; CS₂; MeI / tetrahydrofuran / 20 °C

5.3: n-Bu₃SnH; AIBN / benzene / Heating

With tert.-butyl lithium; diisobutylaluminium hydride; potassium carbonate; caesium carbonate; toluene-4-sulfonic acid; thien-2-yl(cyano)copper lithium; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; acetonitrile; benzene;
DOI:10.1016/j.tetlet.2007.01.024