3-phenylthiopropionic acid S-(2 {3 [2,2,5,5 tertamethyl[1,3]dioxane 4R-carbonyl-amino]propionylamino}ethyl) ester

Base Information

Chemical Name:3-phenylthiopropionic acid S-(2 {3 [2,2,5,5 tertamethyl[1,3]dioxane 4R-carbonyl-amino]propionylamino}ethyl) ester
CAS No.:1333435-19-0
Molecular Formula:C₂₃H₃₄N₂O₅S
Molecular Weight:450.599
Hs Code.:

Synonyms:3-phenylthiopropionic acid S-(2 {3 [2,2,5,5 tertamethyl[1,3]dioxane 4R-carbonyl-amino]propionylamino}ethyl) ester

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Chemical Property of 3-phenylthiopropionic acid S-(2 {3 [2,2,5,5 tertamethyl[1,3]dioxane 4R-carbonyl-amino]propionylamino}ethyl) ester

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Technology Process of 3-phenylthiopropionic acid S-(2 {3 [2,2,5,5 tertamethyl[1,3]dioxane 4R-carbonyl-amino]propionylamino}ethyl) ester

There total 3 articles about 3-phenylthiopropionic acid S-(2 {3 [2,2,5,5 tertamethyl[1,3]dioxane 4R-carbonyl-amino]propionylamino}ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 167308-64-7
3-{[(R)-2,2,5,5-tetramethyl-1,3-dioxan-4-yl]carbonylamino}-1-(2-mercaptoethylamino)-1-propanone

: 23522-73-8
3-phenylpropionic acid 4-chlorophenyl ester

: 1333435-19-0
3-phenylthiopropionic acid S-(2 {3 [2,2,5,5 tertamethyl[1,3]dioxane 4R-carbonyl-amino]propionylamino}ethyl) ester

Guidance literature:: With [Bu₄N][Fe(CO)₃(NO)]; In 1,4-dioxane; at 20 - 80 ℃; for 48h; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.201101073

Reference yield:

: 97723-86-9
3-phenylthiopropionic acid S-4-chlorophenyl ester

: 1333435-19-0
3-phenylthiopropionic acid S-(2 {3 [2,2,5,5 tertamethyl[1,3]dioxane 4R-carbonyl-amino]propionylamino}ethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: [Bu₄N][Fe(CO)₃(NO)] / 1,4-dioxane / 22 h / 80 °C / Molecular sieve

2: [Bu₄N][Fe(CO)₃(NO)] / 1,4-dioxane / 48 h / 20 - 80 °C / Molecular sieve; Inert atmosphere

With [Bu₄N][Fe(CO)₃(NO)]; In 1,4-dioxane;
DOI:10.1002/chem.201101073

Reference yield:

: 501-52-0
3-Phenylpropionic acid

: 1333435-19-0
3-phenylthiopropionic acid S-(2 {3 [2,2,5,5 tertamethyl[1,3]dioxane 4R-carbonyl-amino]propionylamino}ethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

2: [Bu₄N][Fe(CO)₃(NO)] / 1,4-dioxane / 48 h / 20 - 80 °C / Molecular sieve; Inert atmosphere

With dmap; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane;
DOI:10.1002/chem.201101073