C₃₅H₂₃NO₂S

Base Information

Chemical Name:C₃₅H₂₃NO₂S
CAS No.:1422184-07-3
Molecular Formula:C₃₅H₂₃NO₂S
Molecular Weight:521.639
Hs Code.:

C<sub>35</sub>H<sub>23</sub>NO<sub>2</sub>S

Synonyms:C₃₅H₂₃NO₂S

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Chemical Property of C₃₅H₂₃NO₂S

Chemical Property:

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Technology Process of C₃₅H₂₃NO₂S

There total 5 articles about C₃₅H₂₃NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1422184-04-0
C₃₀H₂₀BrNO

: (5-formylthiophen-2-yl)boronic acid

: 1422184-07-3
C₃₅H₂₃NO₂S

Guidance literature:: C₃₀H₂₀BrNO; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 45 ℃; for 1h; Inert atmosphere;

(5-formylthiophen-2-yl)boronic acid; In tetrahydrofuran; water; at 45 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.tet.2012.12.074

Reference yield:

: 36809-26-4
4-N,N-diphenylamino-1-bromobenzene

: 1422184-07-3
C₃₅H₂₃NO₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 °C / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere

2.1: hydrogenchloride / tetrahydrofuran; hexane; water / pH 2 - Ca_. 3 / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 1 h / 45 °C / Inert atmosphere

3.2: 4 h / Inert atmosphere; Reflux

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 1 h / 45 °C / Inert atmosphere

4.2: 4 h / 45 °C / Inert atmosphere

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium carbonate; In tetrahydrofuran; hexane; water; 3.1: |Suzuki Coupling / 3.2: |Suzuki Coupling / 4.1: |Suzuki Coupling / 4.2: |Suzuki Coupling;
DOI:10.1016/j.tet.2012.12.074

Reference yield:

: 201802-67-7
4-(diphenylamino)phenyl boronic acid

: 1422184-07-3
C₃₅H₂₃NO₂S

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 1 h / 45 °C / Inert atmosphere

1.2: 4 h / Inert atmosphere; Reflux

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 1 h / 45 °C / Inert atmosphere

2.2: 4 h / 45 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; 1.1: |Suzuki Coupling / 1.2: |Suzuki Coupling / 2.1: |Suzuki Coupling / 2.2: |Suzuki Coupling;
DOI:10.1016/j.tet.2012.12.074