N-trifluoroacetyl-(S)-phenylalanyl-(R)-(2-(tert-butyldimethylsilyloxy)methylallyl)glycyl-(S)-N-methyl-leucineanilide

Base Information

Chemical Name:N-trifluoroacetyl-(S)-phenylalanyl-(R)-(2-(tert-butyldimethylsilyloxy)methylallyl)glycyl-(S)-N-methyl-leucineanilide
CAS No.:1412908-37-2
Molecular Formula:C₃₆H₅₁F₃N₄O₅Si
Molecular Weight:704.905
Hs Code.:

Synonyms:N-trifluoroacetyl-(S)-phenylalanyl-(R)-(2-(tert-butyldimethylsilyloxy)methylallyl)glycyl-(S)-N-methyl-leucineanilide

Suppliers and Price of N-trifluoroacetyl-(S)-phenylalanyl-(R)-(2-(tert-butyldimethylsilyloxy)methylallyl)glycyl-(S)-N-methyl-leucineanilide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-trifluoroacetyl-(S)-phenylalanyl-(R)-(2-(tert-butyldimethylsilyloxy)methylallyl)glycyl-(S)-N-methyl-leucineanilide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-trifluoroacetyl-(S)-phenylalanyl-(R)-(2-(tert-butyldimethylsilyloxy)methylallyl)glycyl-(S)-N-methyl-leucineanilide

There total 1 articles about N-trifluoroacetyl-(S)-phenylalanyl-(R)-(2-(tert-butyldimethylsilyloxy)methylallyl)glycyl-(S)-N-methyl-leucineanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 950584-19-7
2-(((tert-butyldimethylsilyl)oxy)methyl)allyl ethyl carbonate

: 1412908-27-0
N-trifluoroacetyl-(S)-phenylalanyl-glycyl-(S)-N-methyl-leucineanilide

: 1412908-37-2
N-trifluoroacetyl-(S)-phenylalanyl-(R)-(2-(tert-butyldimethylsilyloxy)methylallyl)glycyl-(S)-N-methyl-leucineanilide

Guidance literature:: N-trifluoroacetyl-(S)-phenylalanyl-glycyl-(S)-N-methyl-leucineanilide; With n-butyllithium; diisopropylamine; zinc(II) chloride; In tetrahydrofuran; at -78 - -40 ℃; for 0.75h; Schlenk technique;

2-(((tert-butyldimethylsilyl)oxy)methyl)allyl ethyl carbonate; With bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine; In tetrahydrofuran; at -78 - 20 ℃; diastereoselective reaction; Schlenk technique;
DOI:10.1039/c2ob26351c DOI:10.1039/c2ob26351c