C₃₃H₃₇NO₄

Base Information

Chemical Name:C₃₃H₃₇NO₄
CAS No.:1384107-28-1
Molecular Formula:C₃₃H₃₇NO₄
Molecular Weight:511.661
Hs Code.:

C<sub>33</sub>H<sub>37</sub>NO<sub>4</sub>

Synonyms:C₃₃H₃₇NO₄

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Chemical Property of C₃₃H₃₇NO₄

Chemical Property:

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Technology Process of C₃₃H₃₇NO₄

There total 9 articles about C₃₃H₃₇NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1384107-27-0
C₃₃H₃₇N₃O₄

: 1384107-28-1
C₃₃H₃₇NO₄

Guidance literature:: With chlorosulfonic acid; In dichloromethane; at -30 ℃; for 6h;
DOI:10.1021/ol301331t

Reference yield:

: 1384107-23-6
C₃₂H₃₇N₃O₅

: 1384107-28-1
C₃₃H₃₇NO₄

Guidance literature:: Multi-step reaction with 5 steps

1: water; toluene-4-sulfonic acid / acetone / 24 h / 70 °C

2: potassium hydroxide / dimethyl sulfoxide / 2 h / 25 °C / Inert atmosphere

3: sodium tetrahydroborate / ethanol / 2 h / 25 °C

4: pyridine; 3-chloro-benzenecarboperoxoic acid / hexane; dichloromethane / -30 - 20 °C

5: chlorosulfonic acid / dichloromethane / 6 h / -30 °C

With pyridine; chlorosulfonic acid; sodium tetrahydroborate; water; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In ethanol; hexane; dichloromethane; dimethyl sulfoxide; acetone; 5: Schmidt reaction;
DOI:10.1021/ol301331t

Reference yield:

: 1384107-25-8
C₃₃H₃₇N₃O₄

: 1384107-28-1
C₃₃H₃₇NO₄

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / ethanol / 2 h / 25 °C

2: pyridine; 3-chloro-benzenecarboperoxoic acid / hexane; dichloromethane / -30 - 20 °C

3: chlorosulfonic acid / dichloromethane / 6 h / -30 °C

With pyridine; chlorosulfonic acid; sodium tetrahydroborate; 3-chloro-benzenecarboperoxoic acid; In ethanol; hexane; dichloromethane; 3: Schmidt reaction;
DOI:10.1021/ol301331t