C₂₆H₃₁IN₂O₆

Base Information

Chemical Name:C₂₆H₃₁IN₂O₆
CAS No.:1016976-38-7
Molecular Formula:C₂₆H₃₁IN₂O₆
Molecular Weight:594.446
Hs Code.:

C<sub>26</sub>H<sub>31</sub>IN<sub>2</sub>O<sub>6</sub>

Synonyms:C₂₆H₃₁IN₂O₆

Suppliers and Price of C₂₆H₃₁IN₂O₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₆H₃₁IN₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₆H₃₁IN₂O₆

There total 16 articles about C₂₆H₃₁IN₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1016976-23-0
C₃₂H₄₅IN₂O₆Si

: 1016976-38-7
C₂₆H₃₁IN₂O₆

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ol800127a

Reference yield:

: 885703-19-5
(3S,4S)-4-N-phthalimido-1,5-hexadiene-3-ol

: 1016976-38-7
C₂₆H₃₁IN₂O₆

Guidance literature:: Multi-step reaction with 12 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 11 h / 20 °C / Inert atmosphere

2: osmium(VIII) oxide; (8a,9R,8′′′a,9′′′R)-9,9′-[(2,5-diphenylpyrimidine-4,6-diyl)bis(oxy)]bis(6′-methoxy-10,11-dihydrocinchonan); methanesulfonamide; sodium hydrogencarbonate; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 6 h / 5 °C / Inert atmosphere

3: nitrogen; methylamine / water / 1 h / 50 °C / 10 Torr / Inert atmosphere

4: sodium hydrogencarbonate / ethyl acetate / 1.5 h / Inert atmosphere

5: dmap; triethylamine; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.03 h / 0 - 20 °C / Inert atmosphere

6: dichloromethane / 1 h / -40 °C / Inert atmosphere

7: caesium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

8: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / Inert atmosphere

9: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

10: acetic acid / chloroform / 12 h / 20 °C / Molecular sieve; Inert atmosphere

11: sodium cyanoborohydride / tetrahydrofuran / 2 h / Inert atmosphere

12: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

With 1H-imidazole; dmap; osmium(VIII) oxide; (8a,9R,8′′′a,9′′′R)-9,9′-[(2,5-diphenylpyrimidine-4,6-diyl)bis(oxy)]bis(6′-methoxy-10,11-dihydrocinchonan); methanesulfonamide; nitrogen; tetrabutyl ammonium fluoride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; caesium carbonate; Dess-Martin periodane; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; methylamine; potassium hexacyanoferrate(III); In tetrahydrofuran; dichloromethane; chloroform; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/chem.201003489

Reference yield:

: 1016976-13-8
3-benzyloxy-4-iodo-5-nitrobenzaldehyde

: 1016976-38-7
C₂₆H₃₁IN₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1: N-iodo-succinimide; potassium carbonate / acetonitrile / 12 h / 5 °C / Inert atmosphere; Darkness

2: iron; acetic acid / tetrahydrofuran; methanol / 3.5 h / 20 °C / Inert atmosphere

3: acetic acid / chloroform / 12 h / 20 °C / Molecular sieve; Inert atmosphere

4: sodium cyanoborohydride / tetrahydrofuran / 2 h / Inert atmosphere

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

With N-iodo-succinimide; tetrabutyl ammonium fluoride; iron; sodium cyanoborohydride; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; chloroform; acetonitrile;
DOI:10.1002/chem.201003489