C₁₃⁽¹³⁾C₂H₂₄O

Base Information

• Chemical Name: C₁₃⁽¹³⁾C₂H₂₄O
• CAS No.: 347367-54-8
• Molecular Formula: C₁₅H₂₄O
• Molecular Weight: 222.333
• Mol file: 347367-54-8.mol

Synonyms:C₁₃⁽¹³⁾C₂H₂₄O

Chemical Property of C₁₃⁽¹³⁾C₂H₂₄O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃⁽¹³⁾C₂H₂₄O

There total 2 articles about C₁₃⁽¹³⁾C₂H₂₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

[10,11-13C2]-(2E,4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate (347367-53-7) → C13(13)C2H24O (347367-54-8)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1002/jlcr.464

Reference yield:

(E)-β-ionone (79-77-6,14901-07-6) → C13(13)C2H24O (347367-54-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / NaH / diethyl ether

2: 99 percent / LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; sodium hydride; In diethyl ether; 1: Wittig-Horner reaction;

DOI:10.1002/jlcr.464

Reference yield: 92.0%

C13(13)C2H24O (347367-54-8) → [10,11-13C2]-(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienal (100187-26-6)

Guidance literature:

With manganese(IV) oxide; In hexane;

DOI:10.1002/jlcr.464

upstream raw materials:

[10,11-13C₂]-(2E,4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate

(E)-β-ionone

Downstream raw materials:

[10,11-13C₂]-(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienal

C₁₆⁽¹³⁾C₂H₂₆O

10,11,14,15-¹³C₄-retinol

10,11,14,15-¹³C₄-retinoic acid ethyl ester

Refernces