6-{5-(diethylamino)-2-[(E)-2-(4-nitrophenyl)-1-ethenyl]phenoxy}-1-hexanol

Base Information

Chemical Name:6-{5-(diethylamino)-2-[(E)-2-(4-nitrophenyl)-1-ethenyl]phenoxy}-1-hexanol
CAS No.:736981-13-8
Molecular Formula:C₂₄H₃₂N₂O₄
Molecular Weight:412.529
Hs Code.:

Synonyms:6-{5-(diethylamino)-2-[(E)-2-(4-nitrophenyl)-1-ethenyl]phenoxy}-1-hexanol

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Chemical Property of 6-{5-(diethylamino)-2-[(E)-2-(4-nitrophenyl)-1-ethenyl]phenoxy}-1-hexanol

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Technology Process of 6-{5-(diethylamino)-2-[(E)-2-(4-nitrophenyl)-1-ethenyl]phenoxy}-1-hexanol

There total 3 articles about 6-{5-(diethylamino)-2-[(E)-2-(4-nitrophenyl)-1-ethenyl]phenoxy}-1-hexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 586972-34-1
4-(diethylamino)-2-[(6-hydroxyhexyl)oxy]benzaldehyde

: 104-03-0
4-nitrobenzeneacetic acid

: 736981-13-8
6-{5-(diethylamino)-2-[(E)-2-(4-nitrophenyl)-1-ethenyl]phenoxy}-1-hexanol

Guidance literature:: With piperidine; In N,N-dimethyl-formamide; at 100 ℃; for 10h;
DOI:10.1021/ma040044i

Reference yield:

: 2009-83-8
6-chloro-1-hexanol

: 736981-13-8
6-{5-(diethylamino)-2-[(E)-2-(4-nitrophenyl)-1-ethenyl]phenoxy}-1-hexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / potassium carbonate / dimethylformamide; toluene / 24 h / Heating

2: 25 percent / piperidine / dimethylformamide / 10 h / 100 °C

With piperidine; potassium carbonate; In N,N-dimethyl-formamide; toluene; 2: Knoevenagel condensation;
DOI:10.1021/ma040044i

Reference yield:

: 17754-90-4
4-(Diethylamino)salicylaldehyde

: 736981-13-8
6-{5-(diethylamino)-2-[(E)-2-(4-nitrophenyl)-1-ethenyl]phenoxy}-1-hexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / potassium carbonate / dimethylformamide; toluene / 24 h / Heating

2: 25 percent / piperidine / dimethylformamide / 10 h / 100 °C

With piperidine; potassium carbonate; In N,N-dimethyl-formamide; toluene; 2: Knoevenagel condensation;
DOI:10.1021/ma040044i