3,6-Diazabicyclo[3.1.1]heptane, 6-(1-oxopropyl)- (9CI)

Base Information

Chemical Name:3,6-Diazabicyclo[3.1.1]heptane, 6-(1-oxopropyl)- (9CI)
CAS No.:869494-18-8
Molecular Formula:C₈H₁₄N₂O
Molecular Weight:154.212
Hs Code.:
Mol file:869494-18-8.mol

Synonyms:3,6-Diazabicyclo[3.1.1]heptane,6-(1-oxopropyl)- (9CI); 6-Propionyl-3,6-diazabicyclo[3.1.1]heptane

Suppliers and Price of 3,6-Diazabicyclo[3.1.1]heptane, 6-(1-oxopropyl)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 3,6-Diazabicyclo[3.1.1]heptane, 6-(1-oxopropyl)- (9CI)

Chemical Property:

PSA：32.34000
LogP:0.23580

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,6-Diazabicyclo[3.1.1]heptane, 6-(1-oxopropyl)- (9CI)

There total 19 articles about 3,6-Diazabicyclo[3.1.1]heptane, 6-(1-oxopropyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 3-benzyl-6-propionyl-3,6-diazabicyclo[3.1.1]heptane

: 869494-18-8
6-propionyl-3,6-diazabicyclo[3.1.1]heptane

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethanol; at 60 ℃; for 7h; under 2327.23 Torr;

Reference yield: 95.0%

: 3-benzyl-6-propionyl-3,6-diazabicyclo[3.1.1]heptane

: 869494-18-8
6-propionyl-3,6-diazabicyclo[3.1.1]heptane

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 60 ℃; for 7h; under 2280 Torr;
DOI:10.1016/j.bmc.2005.09.045

Reference yield:

: (1R,5S)-3-benzyl-3,6-diazabicyclo[3.1.1]heptane

: 869494-18-8
6-propionyl-3,6-diazabicyclo[3.1.1]heptane

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / CH₂Cl₂ / 1 h / Heating

2: 95 percent / hydrogen / Pd/C / ethanol / 7 h / 60 °C / 2280 Torr

With hydrogen; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1016/j.bmc.2005.09.045