(R)-3-(Dimethyl-phenyl-silanyl)-pentanedioic acid tert-butyl ester methyl ester

Base Information

Chemical Name:(R)-3-(Dimethyl-phenyl-silanyl)-pentanedioic acid tert-butyl ester methyl ester
CAS No.:223117-82-6
Molecular Formula:C₁₈H₂₈O₄Si
Molecular Weight:336.503
Hs Code.:

Synonyms:(R)-3-(Dimethyl-phenyl-silanyl)-pentanedioic acid tert-butyl ester methyl ester

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Chemical Property of (R)-3-(Dimethyl-phenyl-silanyl)-pentanedioic acid tert-butyl ester methyl ester

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Technology Process of (R)-3-(Dimethyl-phenyl-silanyl)-pentanedioic acid tert-butyl ester methyl ester

There total 3 articles about (R)-3-(Dimethyl-phenyl-silanyl)-pentanedioic acid tert-butyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 223117-76-8
(3R)-benzyl tert-butyl 3-[dimethyl(phenyl)silyl]pentane-1,5-dioate

: 223117-82-6
(R)-3-(Dimethyl-phenyl-silanyl)-pentanedioic acid tert-butyl ester methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethyl acetate / 15 h

2: diethyl ether

With hydrogen; palladium on activated charcoal; In diethyl ether; ethyl acetate;
DOI:10.1039/a808840c

Reference yield:

: 223118-72-7
(R)-5-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-3-(dimethyl-phenyl-silanyl)-5-oxo-pentanoic acid tert-butyl ester

: 223117-82-6
(R)-3-(Dimethyl-phenyl-silanyl)-pentanedioic acid tert-butyl ester methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / Ti(OBn)4 / 24 h / 75 °C

2: H₂ / 10percent Pd/C / ethyl acetate / 15 h

3: diethyl ether

With tetrabutoxytitanium; hydrogen; palladium on activated charcoal; In diethyl ether; ethyl acetate;
DOI:10.1039/a808840c