sodium 1-<<(R)-3-(benzyloxycarbonyl)-5-oxo-4-oxazolidinyl>propionyl>indoline-2(S)-carboxylate

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Chemical Name:sodium 1-<<(R)-3-(benzyloxycarbonyl)-5-oxo-4-oxazolidinyl>propionyl>indoline-2(S)-carboxylate
CAS No.:97975-58-1
Molecular Formula:C₂₃H₂₁N₂O₇*Na
Molecular Weight:460.419
Hs Code.:

Synonyms:sodium 1-<<(R)-3-(benzyloxycarbonyl)-5-oxo-4-oxazolidinyl>propionyl>indoline-2(S)-carboxylate

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Chemical Property of sodium 1-<<(R)-3-(benzyloxycarbonyl)-5-oxo-4-oxazolidinyl>propionyl>indoline-2(S)-carboxylate

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Technology Process of sodium 1-<<(R)-3-(benzyloxycarbonyl)-5-oxo-4-oxazolidinyl>propionyl>indoline-2(S)-carboxylate

There total 3 articles about sodium 1-<<(R)-3-(benzyloxycarbonyl)-5-oxo-4-oxazolidinyl>propionyl>indoline-2(S)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 97975-62-7
dimethylaminoethyl 1-<<(R)-3-(benzyloxycarbonyl)-5-oxo-4-oxazolidinyl>propionyl>indoline-2(S)-carboxylate

: 97975-58-1
sodium 1-<<(R)-3-(benzyloxycarbonyl)-5-oxo-4-oxazolidinyl>propionyl>indoline-2(S)-carboxylate

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; for 2h;
DOI:10.1021/jm00149a011

Reference yield:

: 97975-57-0
(4R)-4-(2-Carboxyethyl)-3-[(phenylmethoxy)carbonyl]oxazolidin-5-one

: 97975-58-1
sodium 1-<<(R)-3-(benzyloxycarbonyl)-5-oxo-4-oxazolidinyl>propionyl>indoline-2(S)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / 15 h / Ambient temperature

2: 53 percent / 1 N NaOH / tetrahydrofuran / 2 h

With sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00149a011

Reference yield:

: 97975-30-9
(S)-2,3-Dihydro-1H-indole-2-carboxylic acid 2-dimethylamino-ethyl ester

: 97975-58-1
sodium 1-<<(R)-3-(benzyloxycarbonyl)-5-oxo-4-oxazolidinyl>propionyl>indoline-2(S)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / 15 h / Ambient temperature

2: 53 percent / 1 N NaOH / tetrahydrofuran / 2 h

With sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00149a011