(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-S-(1,2,4-triazol-3-yl)-β-D-ribofuranoside

Base Information

Chemical Name:(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-S-(1,2,4-triazol-3-yl)-β-D-ribofuranoside
CAS No.:1356821-72-1
Molecular Formula:C₂₀H₂₆N₄O₈S
Molecular Weight:482.514
Hs Code.:

Synonyms:(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-S-(1,2,4-triazol-3-yl)-β-D-ribofuranoside

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Chemical Property of (3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-S-(1,2,4-triazol-3-yl)-β-D-ribofuranoside

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Technology Process of (3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-S-(1,2,4-triazol-3-yl)-β-D-ribofuranoside

There total 5 articles about (3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-S-(1,2,4-triazol-3-yl)-β-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1356821-71-0
(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-S-(1,2,4-triazol-3-yl)-2,3-O-cyclopentylidene-β-D-ribofuranoside

: 1356821-72-1
(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-S-(1,2,4-triazol-3-yl)-β-D-ribofuranoside

Guidance literature:: With acetic acid; at 40 ℃; for 48h;
DOI:10.1016/j.ejmech.2011.10.028

Reference yield:

: allyl 2,3-O-cyclopentylidene-β-D-ribofuranoside

: 1356821-72-1
(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-S-(1,2,4-triazol-3-yl)-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / 20 °C / Inert atmosphere

2.1: sodium ethanolate / ethanol / 0.17 h / 50 °C

2.2: 18 h / 50 °C / Inert atmosphere

3.1: acetic acid / 24 h / 55 °C

4.1: chloroamine-T / water; tert-butyl alcohol / 2 h / 45 °C

5.1: acetic acid / 48 h / 40 °C

With pyridine; sodium ethanolate; chloroamine-T; acetic acid; In ethanol; water; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2011.10.028

Reference yield:

: 1356821-68-5
allyl 2,3-O-cyclopentylidene-5-tosyl-β-D-ribofuranoside

: 1356821-72-1
(3-(3,4,5-trimethoxyphenyl)-isoxazolin-5-yl)methyl 5-deoxy-5-S-(1,2,4-triazol-3-yl)-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium ethanolate / ethanol / 0.17 h / 50 °C

1.2: 18 h / 50 °C / Inert atmosphere

2.1: acetic acid / 24 h / 55 °C

3.1: chloroamine-T / water; tert-butyl alcohol / 2 h / 45 °C

4.1: acetic acid / 48 h / 40 °C

With sodium ethanolate; chloroamine-T; acetic acid; In ethanol; water; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2011.10.028