2-((3-(((tert-butoxycarbonyl)amino)methyl)benzyl)amino)acetic acid hydrochloride

Base Information

Chemical Name:2-((3-(((tert-butoxycarbonyl)amino)methyl)benzyl)amino)acetic acid hydrochloride
CAS No.:1432623-68-1
Molecular Formula:C₁₅H₂₂N₂O₄*ClH
Molecular Weight:330.812
Hs Code.:

Synonyms:2-((3-(((tert-butoxycarbonyl)amino)methyl)benzyl)amino)acetic acid hydrochloride

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Chemical Property of 2-((3-(((tert-butoxycarbonyl)amino)methyl)benzyl)amino)acetic acid hydrochloride

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Technology Process of 2-((3-(((tert-butoxycarbonyl)amino)methyl)benzyl)amino)acetic acid hydrochloride

There total 1 articles about 2-((3-(((tert-butoxycarbonyl)amino)methyl)benzyl)amino)acetic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1432623-67-0
ethyl 2-((3-(((tert-butoxycarbonyl)amino)methyl)benzyl)amino)acetate

: 1432623-68-1
2-((3-(((tert-butoxycarbonyl)amino)methyl)benzyl)amino)acetic acid hydrochloride

Guidance literature:: ethyl 2-((3-(((tert-butoxycarbonyl)amino)methyl)benzyl)amino)acetate; With sodium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃; for 0.5h;

With hydrogenchloride; In water;
DOI:10.1021/ja403539t

Reference yield: 54.0%

: dysprosium(III) chloride hexahydrate

: 1432623-68-1
2-((3-(((tert-butoxycarbonyl)amino)methyl)benzyl)amino)acetic acid hydrochloride

: 120-46-7,61346-73-4
1,3-diphenylpropanedione

: [{Dy₁₅(μ₃-OH)₂₀(2-[{3-(((tert-butoxycarbonyl)amino)methyl)benzyl}amino]acetate)₁₀(dibenzoylmethanide)₁₀Cl}Cl₄]

Guidance literature:: 2-((3-(((tert-butoxycarbonyl)amino)methyl)benzyl)amino)acetic acid hydrochloride; With potassium tert-butylate; In methanol; at 20 ℃; for 0.5h;

dysprosium(III) chloride hexahydrate; In methanol; at 20 ℃; for 0.75h;

1,3-diphenylpropanedione; In methanol; at 20 ℃;
DOI:10.1002/chem.201405569

Reference yield: 40.0%

: europium(III) chloride hexahydrate

: 1432623-68-1
2-((3-(((tert-butoxycarbonyl)amino)methyl)benzyl)amino)acetic acid hydrochloride

: 120-46-7,61346-73-4
1,3-diphenylpropanedione

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: [Eu₁₅(μ3-OH)₂₀(2-[{3-(((tert-butoxycarbonyl)-amino)methyl)benzyl}amino]acetate)₁₀(dibenzoylmethane)₁₀Cl]Cl₄

Guidance literature:: 2-((3-(((tert-butoxycarbonyl)amino)methyl)benzyl)amino)acetic acid hydrochloride; With potassium tert-butylate; In methanol; at 20 ℃; for 0.5h;

europium(III) chloride hexahydrate; In methanol;

1,3-diphenylpropanedione; N,N-dimethyl-formamide;
DOI:10.1021/ja403539t