C₁₈H₁₁ClOS

Base Information

Chemical Name:C₁₈H₁₁ClOS
CAS No.:1401613-06-6
Molecular Formula:C₁₈H₁₁ClOS
Molecular Weight:310.804
Hs Code.:

Synonyms:C₁₈H₁₁ClOS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₁₁ClOS

Chemical Property:

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Technology Process of C₁₈H₁₁ClOS

There total 1 articles about C₁₈H₁₁ClOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1003-09-4
2-bromothiophene

: 4889-69-4
3-(4-chlorophenyl)phthalide

: 1401613-06-6
C₁₈H₁₁ClOS

Guidance literature:: With magnesium;
DOI:10.1021/jo301410w

Reference yield: 86.0%

: 1401613-06-6
C₁₈H₁₁ClOS

: 208-96-8,25036-01-5
acenaphthylene

: 2-[12-(4-chlorophenyl)benzo[k]fluoranthen-7-yl]thiophene

Guidance literature:: C₁₈H₁₁ClOS; acenaphthylene; In 5,5-dimethyl-1,3-cyclohexadiene; Reflux; Inert atmosphere;

With toluene-4-sulfonic acid; In 5,5-dimethyl-1,3-cyclohexadiene; for 8h; Reflux; Inert atmosphere;
DOI:10.1002/ejoc.201701137

Reference yield:

: 1401613-06-6
C₁₈H₁₁ClOS

: 2-(4-(4-chlorophenyl)naphthalen-1-yl)thiophene

Guidance literature:: Multi-step reaction with 2 steps

1: 5,5-dimethyl-1,3-cyclohexadiene / 6 h / Inert atmosphere; Reflux

2: trifluorormethanesulfonic acid / dichloromethane / 0.17 h / 0 - 20 °C / Inert atmosphere

With trifluorormethanesulfonic acid; In 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; 1: |Diels-Alder Cycloaddition;
DOI:10.1021/acs.orglett.7b03686