Toluene-4-sulfonic acid bicyclo[6.2.2]dodeca-1⁽¹⁰⁾,8,11-trien-9-ylmethyl ester

Base Information

Chemical Name:Toluene-4-sulfonic acid bicyclo[6.2.2]dodeca-1⁽¹⁰⁾,8,11-trien-9-ylmethyl ester
CAS No.:129786-05-6
Molecular Formula:C₂₀H₂₄O₃S
Molecular Weight:344.475
Hs Code.:

Toluene-4-sulfonic acid bicyclo[6.2.2]dodeca-1<sup>(10)</sup>,8,11-trien-9-ylmethyl ester

Synonyms:Toluene-4-sulfonic acid bicyclo[6.2.2]dodeca-1⁽¹⁰⁾,8,11-trien-9-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Toluene-4-sulfonic acid bicyclo[6.2.2]dodeca-1⁽¹⁰⁾,8,11-trien-9-ylmethyl ester

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Technology Process of Toluene-4-sulfonic acid bicyclo[6.2.2]dodeca-1⁽¹⁰⁾,8,11-trien-9-ylmethyl ester

There total 2 articles about Toluene-4-sulfonic acid bicyclo[6.2.2]dodeca-1⁽¹⁰⁾,8,11-trien-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 129786-04-5
8-hydroxymethyl<6>paracyclophane

: 98-59-9
p-toluenesulfonyl chloride

: 129786-05-6
Toluene-4-sulfonic acid bicyclo[6.2.2]dodeca-1⁽¹⁰⁾,8,11-trien-9-ylmethyl ester

Guidance literature:: With n-butyllithium; In tetrahydrofuran;
DOI:10.1021/ja00177a013

Reference yield:

: 84538-15-8,97373-08-5,97373-10-9
(+/-)-<6>Paracyclophan-8-carbonsaeure-methylester

: 129786-05-6
Toluene-4-sulfonic acid bicyclo[6.2.2]dodeca-1⁽¹⁰⁾,8,11-trien-9-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / LAH / diethyl ether

2: 84 percent / BuLi / tetrahydrofuran

With lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00177a013