Technology Process of C39H31BF2N2
There total 6 articles about C39H31BF2N2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine;
In
toluene;
at 20 ℃;
for 0.5h;
DOI:10.1016/j.tet.2011.03.016
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium hydroxide / ethylene glycol / 2 h / 175 °C / Inert atmosphere; Darkness
2.1: trifluoroacetic acid / dichloromethane / Reflux; Inert atmosphere
2.2: 20 °C / Inert atmosphere
3.1: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / toluene / 0.5 h / 20 °C
With
boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; potassium hydroxide;
In
dichloromethane; ethylene glycol; toluene;
DOI:10.1016/j.tet.2011.03.016
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trifluoroacetic acid / dichloromethane / Reflux; Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / toluene / 0.5 h / 20 °C
With
boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; toluene;
DOI:10.1016/j.tet.2011.03.016