1-Hydroxy-8-methoxy-2-[3-(3,4,5-trimethoxy-phenyl)-propyl]-anthraquinone

Base Information

Chemical Name:1-Hydroxy-8-methoxy-2-[3-(3,4,5-trimethoxy-phenyl)-propyl]-anthraquinone
CAS No.:155920-73-3
Molecular Formula:C₂₇H₂₆O₇
Molecular Weight:462.499
Hs Code.:

Synonyms:1-Hydroxy-8-methoxy-2-[3-(3,4,5-trimethoxy-phenyl)-propyl]-anthraquinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Hydroxy-8-methoxy-2-[3-(3,4,5-trimethoxy-phenyl)-propyl]-anthraquinone

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Technology Process of 1-Hydroxy-8-methoxy-2-[3-(3,4,5-trimethoxy-phenyl)-propyl]-anthraquinone

There total 2 articles about 1-Hydroxy-8-methoxy-2-[3-(3,4,5-trimethoxy-phenyl)-propyl]-anthraquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53560-26-2
3-(3,4,5-trimethoxyphenyl)propan-1-ol

: 155920-73-3
1-Hydroxy-8-methoxy-2-[3-(3,4,5-trimethoxy-phenyl)-propyl]-anthraquinone

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / pyridinium chlorochromate / CH₂Cl₂ / 1.5 h

2: 1.) 1.5percent aq. NaOH, aq. Na₂S₂O₄ / 1.) 50 deg C, 15 min, 2.) 90 deg C, 3 h

With sodium hydroxide; sodium dithionite; pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/jm00037a017

Reference yield:

: 5539-66-2
1-hydroxy-8-methoxyanthraquinone

: 121667-78-5
3-(3',4',5'-trimethoxyphenyl)propanal

: 155920-73-3
1-Hydroxy-8-methoxy-2-[3-(3,4,5-trimethoxy-phenyl)-propyl]-anthraquinone

Guidance literature:: With sodium hydroxide; sodium dithionite; Yield given. Multistep reaction; 1.) 50 deg C, 15 min, 2.) 90 deg C, 3 h;
DOI:10.1021/jm00037a017