(2-methoxy-5-phenanthren-9-ylfuran-3-yl)(diphenyl)thiophen-2-ylphosphonium tetrafluoroborate

Base Information

Chemical Name:(2-methoxy-5-phenanthren-9-ylfuran-3-yl)(diphenyl)thiophen-2-ylphosphonium tetrafluoroborate
CAS No.:1448326-02-0
Molecular Formula:BF₄*C₃₅H₂₆O₂PS
Molecular Weight:628.435
Hs Code.:

Synonyms:(2-methoxy-5-phenanthren-9-ylfuran-3-yl)(diphenyl)thiophen-2-ylphosphonium tetrafluoroborate

Suppliers and Price of (2-methoxy-5-phenanthren-9-ylfuran-3-yl)(diphenyl)thiophen-2-ylphosphonium tetrafluoroborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-methoxy-5-phenanthren-9-ylfuran-3-yl)(diphenyl)thiophen-2-ylphosphonium tetrafluoroborate

Chemical Property:

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Technology Process of (2-methoxy-5-phenanthren-9-ylfuran-3-yl)(diphenyl)thiophen-2-ylphosphonium tetrafluoroborate

There total 2 articles about (2-methoxy-5-phenanthren-9-ylfuran-3-yl)(diphenyl)thiophen-2-ylphosphonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 32870-98-7
9-ethynylphenanthrene

: 1448325-77-6
[diphenyl(thiophen-2-yl)phosphonio](methoxycarbonyl)

: 1448326-00-8
methyl 4-(4-methoxyphenyl)-7,7-diphenyl-7λ⁵-phosphinino[2,3-b]thiophene-6-carboxylate

: 1448326-02-0
(2-methoxy-5-phenanthren-9-ylfuran-3-yl)(diphenyl)thiophen-2-ylphosphonium tetrafluoroborate

Guidance literature:: In dichloromethane;
DOI:10.1016/j.tet.2013.06.066

Reference yield:

: 1448325-74-3
methyl [diphenyl(thiophen-2-yl)-λ⁵-phosphanylidene]acetate

: 1448326-00-8
methyl 4-(4-methoxyphenyl)-7,7-diphenyl-7λ⁵-phosphinino[2,3-b]thiophene-6-carboxylate

: 1448326-02-0
(2-methoxy-5-phenanthren-9-ylfuran-3-yl)(diphenyl)thiophen-2-ylphosphonium tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 1 h / 0 - 5 °C

2: dichloromethane

In methanol; dichloromethane;
DOI:10.1016/j.tet.2013.06.066