3-phenyl-1H-dibenzo[e,g]indazole

Base Information

Chemical Name:3-phenyl-1H-dibenzo[e,g]indazole
CAS No.:37944-54-0
Molecular Formula:C₂₁H₁₄N₂
Molecular Weight:294.356
Hs Code.:

Synonyms:3-phenyl-1H-dibenzo[e,g]indazole

Suppliers and Price of 3-phenyl-1H-dibenzo[e,g]indazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of 3-phenyl-1H-dibenzo[e,g]indazole

Chemical Property:

Vapor Pressure:6.17E-13mmHg at 25°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-phenyl-1H-dibenzo[e,g]indazole

There total 5 articles about 3-phenyl-1H-dibenzo[e,g]indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 117745-96-7
9-phenylethynylfluoren-9-ol

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 37944-54-0
3-phenyl-1H-dibenzo[e,g]indazole

Guidance literature:: 9-phenylethynylfluoren-9-ol; toluene-4-sulfonic acid hydrazide; With iron(III) chloride; In chlorobenzene; at 60 ℃; for 1h;

With caesium carbonate; In chlorobenzene; at 100 ℃; for 3h; regioselective reaction;
DOI:10.1002/chem.201204322

Reference yield:

: 84-11-7
9,10-phenanthrenequinone

: 37944-54-0
3-phenyl-1H-dibenzo[e,g]indazole

Guidance literature:: Multi-step reaction with 4 steps

1: 37 percent / benzene / 45 h / Heating

2: 100 percent / KOH / ethanol; H₂O / 1.5 h / Heating

3: 63 percent / glacial acetic acid / 2 h / Heating

4: 36 percent / 100percent NH₂NH₂*H₂O / diethyl ether / 60 h / Ambient temperature

With potassium hydroxide; hydrazine hydrate; acetic acid; In diethyl ether; ethanol; water; benzene;

Reference yield:

: 10-{[(E)-Methylimino]-phenyl-methyl}-phenanthren-9-ol

: 37944-54-0
3-phenyl-1H-dibenzo[e,g]indazole

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / glacial acetic acid / 2 h / Heating

2: 36 percent / 100percent NH₂NH₂*H₂O / diethyl ether / 60 h / Ambient temperature

With hydrazine hydrate; acetic acid; In diethyl ether;