{(1R,2R)-3-((S)-7-Benzyloxymethyl-1,6-dioxa-spiro[4.5]dec-9-en-2-yl)-1-[2-(4-methoxy-benzyloxy)-ethyl]-2-methyl-propoxy}-tert-butyl-diphenyl-silane

Base Information

• Chemical Name: {(1R,2R)-3-((S)-7-Benzyloxymethyl-1,6-dioxa-spiro[4.5]dec-9-en-2-yl)-1-[2-(4-methoxy-benzyloxy)-ethyl]-2-methyl-propoxy}-tert-butyl-diphenyl-silane
• CAS No.: 862995-02-6
• Molecular Formula: C₄₆H₅₈O₆Si
• Molecular Weight: 735.048

Synonyms:{(1R,2R)-3-((S)-7-Benzyloxymethyl-1,6-dioxa-spiro[4.5]dec-9-en-2-yl)-1-[2-(4-methoxy-benzyloxy)-ethyl]-2-methyl-propoxy}-tert-butyl-diphenyl-silane

Chemical Property of {(1R,2R)-3-((S)-7-Benzyloxymethyl-1,6-dioxa-spiro[4.5]dec-9-en-2-yl)-1-[2-(4-methoxy-benzyloxy)-ethyl]-2-methyl-propoxy}-tert-butyl-diphenyl-silane

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Technology Process of {(1R,2R)-3-((S)-7-Benzyloxymethyl-1,6-dioxa-spiro[4.5]dec-9-en-2-yl)-1-[2-(4-methoxy-benzyloxy)-ethyl]-2-methyl-propoxy}-tert-butyl-diphenyl-silane

There total 2 articles about {(1R,2R)-3-((S)-7-Benzyloxymethyl-1,6-dioxa-spiro[4.5]dec-9-en-2-yl)-1-[2-(4-methoxy-benzyloxy)-ethyl]-2-methyl-propoxy}-tert-butyl-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(5R,6S)-1-((2S,6S)-6-Benzyloxymethyl-5,6-dihydro-2H-pyran-2-yl)-6-(tert-butyl-diphenyl-silanyloxy)-7-[2-(4-methoxy-phenyl)-ethoxy]-5-methyl-heptan-3-ol → {(1R,2R)-3-((S)-7-Benzyloxymethyl-1,6-dioxa-spiro[4.5]dec-9-en-2-yl)-1-[2-(4-methoxy-benzyloxy)-ethyl]-2-methyl-propoxy}-tert-butyl-diphenyl-silane (862995-02-6)

Guidance literature:

With [bis(acetoxy)iodo]benzene; iodine; In cyclohexane; at 20 ℃; Irradiation;

DOI:10.1021/ol051260u

Reference yield: 86.0%

(3SR,5R,6R)-1-{(5RS,6S)-6-[(benzyloxy)methyl]-5,6-dihydro-2H-pyran-2-yl}-6-[tert-butyl(diphenyl)silyl]oxy-8-[(4-methoxybenzyl)oxy]-5-methyl-3-octanol → {(1R,2R)-3-((S)-7-Benzyloxymethyl-1,6-dioxa-spiro[4.5]dec-9-en-2-yl)-1-[2-(4-methoxy-benzyloxy)-ethyl]-2-methyl-propoxy}-tert-butyl-diphenyl-silane (862995-02-6)

Guidance literature:

With [bis(acetoxy)iodo]benzene; iodine; In cyclohexane; at 20 ℃; for 2h; Irradiation;

DOI:10.1039/b604334h

Reference yield: 82.0%

{(1R,2R)-3-((S)-7-Benzyloxymethyl-1,6-dioxa-spiro[4.5]dec-9-en-2-yl)-1-[2-(4-methoxy-benzyloxy)-ethyl]-2-methyl-propoxy}-tert-butyl-diphenyl-silane (862995-02-6) → (2R,3R)-1-{(5RS,7S)-7-[(benzyloxy)methyl]-1,6-dioxaspiro[4.5]dec-9-en-7-yl}-5-[(4-methoxybenzyl)oxy]-2-methyl-3-pentanol (901775-15-3)

Guidance literature:

With tetrabutyl ammonium fluoride; In N,N-dimethyl-formamide; at 80 ℃;

DOI:10.1021/ol051260u

Downstream raw materials:

(2R,3R)-1-{(5RS,7S)-7-[(benzyloxy)methyl]-1,6-dioxaspiro[4.5]dec-9-en-7-yl}-5-[(4-methoxybenzyl)oxy]-2-methyl-3-pentanol

(2R,3R,5S,7R,9S,11R,12R)-9-[(benzyloxy)methyl]-2-[2-[(4-methoxybenzyl)oxy]ethyl]-3-methyl-1,6,8-trioxadispiro[4.1.5.2]-11,12-epoxytetradecane

(2R,3R,5S,7R,9S,12R)-9-[(benzyloxy)methyl]-2-[2-[(4-methoxybenzyl)oxy]ethyl]-3-methyl-1,6,8-trioxadispiro[4.1.5.2]tetradecan-12-ol

(2R,3R,5S,7R,9S)-9-[(benzyloxy)methyl]-2-[2-[(4-methoxybenzyl)oxy]ethyl]-3-methyl-1,6,8-trioxadispiro[4.1.5.2]tetradecan-12-one

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