(6 RS)-1,2-O-benzylidene-β-L-ido-1,4;3,6-dialdodifuranose

Base Information

Chemical Name:(6 RS)-1,2-O-benzylidene-β-L-ido-1,4;3,6-dialdodifuranose
CAS No.:73892-52-1
Molecular Formula:C₁₃H₁₄O₆
Molecular Weight:266.251
Hs Code.:

Synonyms:(6 RS)-1,2-O-benzylidene-β-L-ido-1,4;3,6-dialdodifuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (6 RS)-1,2-O-benzylidene-β-L-ido-1,4;3,6-dialdodifuranose

Chemical Property:

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Technology Process of (6 RS)-1,2-O-benzylidene-β-L-ido-1,4;3,6-dialdodifuranose

There total 6 articles about (6 RS)-1,2-O-benzylidene-β-L-ido-1,4;3,6-dialdodifuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73351-55-0,73925-74-3
6-O-acetyl-5-O-benzoyl-1,2-O-benzylidene-(6S)-β-L-ido-hexodialdo-1,4:6,3-difuranose

: 73892-52-1
1,2-O-benzylidene-6S-β-L-ido-hexodialdo-1,4:6,3-difuranose

: 73892-52-1
1,2-O-benzylidene-6R-β-L-ido-hexodialdo-1,4:6,3-difuranose

Guidance literature:: With Amberlite IR-120(H⁽¹⁺⁾) resin; sodium methylate; Amberlite IR-120(H⁽¹⁺⁾) resin; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) methanol, 1 h, RT;
DOI:10.1016/S0008-6215(00)85313-6

Reference yield:

: 73351-55-0,73925-74-3
6-O-acetyl-5-O-benzoyl-1,2-O-benzylidene-(6S)-β-L-ido-hexodialdo-1,4:6,3-difuranose

: 73892-52-1
1,2-O-benzylidene-6S-β-L-ido-hexodialdo-1,4:6,3-difuranose

: 73892-52-1
1,2-O-benzylidene-6R-β-L-ido-hexodialdo-1,4:6,3-difuranose

Guidance literature:: With Amberlite IR-120(H⁽¹⁺⁾) resin; sodium methylate; Amberlite IR-120(H⁽¹⁺⁾) resin; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) methanol, 1 h, RT;
DOI:10.1016/S0008-6215(00)85313-6

Reference yield:

: 72521-48-3,72581-27-2,73925-72-1
Toluene-4-sulfonic acid (3aR,3bS,6S,6aS,7aR)-5-hydroxy-2-phenyl-hexahydro-furo[2',3':4,5]furo[2,3-d][1,3]dioxol-6-yl ester

: 73892-52-1
1,2-O-benzylidene-6S-β-L-ido-hexodialdo-1,4:6,3-difuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) triethylamine; 2.) methanol / 1.) chloroform, 2 h, RT; 2.) 15 min, chloroform

2: 1.) Dowex-1 X₁ (AcO^(1-)) resin; 2.) methanol / 1.) 30 h, reflux; 2.) 1 h, reflux

3: 1.) NaOMe / 2.) Amberlite IR-120(H⁽¹⁺⁾) resin / 1.) methanol, 1 h, RT

With methanol; Dowex-1 X₁ (AcO^(1-)) resin; sodium methylate; triethylamine; Amberlite IR-120(H⁽¹⁺⁾) resin;
DOI:10.1016/S0008-6215(00)85313-6