Technology Process of C16H16O
There total 6 articles about C16H16O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; caesium carbonate; johnphos;
In
toluene;
at 90 ℃;
Inert atmosphere;
Schlenk technique;
DOI:10.1002/jhet.4158
- Guidance literature:
-
With
triethylsilane; boron trifluoride diethyl etherate;
In
dichloromethane;
at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2008.03.003
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium chloride / dimethyl sulfoxide; water / 18 h / 160 °C / Sealed tube; Inert atmosphere
2: lithium aluminium tetrahydride / diethyl ether / 2 h / Inert atmosphere; Cooling
3: caesium carbonate; palladium diacetate; johnphos / toluene / 90 °C / Inert atmosphere; Schlenk technique
With
lithium aluminium tetrahydride; palladium diacetate; caesium carbonate; sodium chloride; johnphos;
In
diethyl ether; water; dimethyl sulfoxide; toluene;
1: |Krapcho Dealkoxycarbonylation / 3: |Buchwald-Hartwig Coupling;
DOI:10.1002/jhet.4158