2-benzyl-3-methoxycarbonyl-1-methyl-3,4-dihydro-9H-pyrido<3,4-b>indolium iodide

Base Information

Chemical Name:2-benzyl-3-methoxycarbonyl-1-methyl-3,4-dihydro-9H-pyrido<3,4-b>indolium iodide
CAS No.:104331-01-3
Molecular Formula:C₂₁H₂₁N₂O₂*I
Molecular Weight:460.314
Hs Code.:

Synonyms:2-benzyl-3-methoxycarbonyl-1-methyl-3,4-dihydro-9H-pyrido<3,4-b>indolium iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzyl-3-methoxycarbonyl-1-methyl-3,4-dihydro-9H-pyrido<3,4-b>indolium iodide

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Technology Process of 2-benzyl-3-methoxycarbonyl-1-methyl-3,4-dihydro-9H-pyrido<3,4-b>indolium iodide

There total 2 articles about 2-benzyl-3-methoxycarbonyl-1-methyl-3,4-dihydro-9H-pyrido<3,4-b>indolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 104331-04-6
N^α-benzyl-N^α-methylthiocarbonyltryptophan methyl ester

: 104331-01-3
2-benzyl-3-methoxycarbonyl-1-methyl-3,4-dihydro-9H-pyrido<3,4-b>indolium iodide

Guidance literature:: With methyl iodide; In dichloromethane; for 24h; Heating;
DOI:10.1248/cpb.33.3237

Reference yield:

: 104331-08-0
2-(Acetyl-benzyl-amino)-3-(1H-indol-3-yl)-propionic acid methyl ester

: 104331-01-3
2-benzyl-3-methoxycarbonyl-1-methyl-3,4-dihydro-9H-pyrido<3,4-b>indolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / Lawesson's reagent / 1,2-dimethoxy-ethane / 3 h / Ambient temperature

2: 62 percent / CH₃I / CH₂Cl₂ / 24 h / Heating

With Lawessons reagent; methyl iodide; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1248/cpb.33.3237